From (PHENYLTHIO)NITROMETHANE, Collective Volume 8 p. 550, Annual Volume 68 p. 8

Caution: Thiophenol (stench!!) and sulfuryl chloride are highly toxic. Steps A and B should be carried out in an efficient fume hood while wearing gloves and adequate eye protection. Sodium nitromethylate is explosive when dry and should be handled only as a slurry.

From VINYL SULFIDES FROM THIOACETALS WITH COPPER(I) TRIFLUOROMETHANESULFONATE: (Z)-2-METHOXY-1-PHENYLTHIO-1,3-BUTADIENE, Collective Volume 6 p. 737, Annual Volume 59 p. 202

Caution! Part A should be carried out in an efficient hood to minimize exposure to the foul-smelling thiophenol.

From SECONDARY AND TERTIARY ALKYL KETONES FROM CARBOXYLIC ACID CHLORIDES AND LITHIUM PHENYLTHIO(ALKYL)CUPRATE REAGENTS: tert-BUTYL PHENYL KETONE, Collective Volume 6 p. 248, Annual Volume 55 p. 122

Caution! Since the odor of the thiophenol (benzenethiol) used in this preparation is unpleasant, both steps of this preparation should be conducted in a hood and the glassware used should be washed before it is removed from the hood.

IRIDIUM-CATALYZED SYNTHESIS OF VINYL ETHERS FROM ALCOHOLS AND VINYL ACETATE
Submitted by: Tomotaka Hirabayashi, Satoshi Sakaguchi, and Yasutaka Ishii
Published in Collective Volume 11 p. 631, Annual Volume 82 p. 55

PHENYLSULFENYLATION OF NONACTIVATED δ-CARBON ATOM BY PHOTOLYSIS OF ALKYL BENZENESULFENATES: PREPARATION OF 2-PHENYLTHIO-5-HEPTANOL
Submitted by: Goran Petrovic, Radomir N. Saicic, and Živorad Cekovic
Published in Collective Volume 11 p. 121, Annual Volume 81 p. 244

MILD AND SELECTIVE OXIDATION OF SULFUR COMPOUNDS IN TRIFLUOROETHANOL: DIPHENYL DISULFIDE AND METHYL PHENYL SULFOXIDE
Submitted by: Kabayadi S. Ravikumar, Venkitasamy Kesavan, Benoit Crousse, Danièle Bonnet-Delpon, and Jean-Pierre Bégué
Published in Collective Volume 11 p. 135, Annual Volume 80 p. 184

PREPARATION OF SECONDARY AMINES FROM PRIMARY AMINES VIA 2-NITROBENZENESULFONAMIDES: N-(4-METHOXYBENZYL)-3-PHENYLPROPYLAMINE
Submitted by: Wataru Kurosawa, Toshiyuki Kan, and Tohru Fukuyama
Published in Collective Volume 10 p. 482, Annual Volume 79 p. 186

DIETHYL [(PHENYLSULFONYL)METHYL]PHOSPHONATE
Submitted by: D. Enders, S. von Berg, and B. Jandeleit
Published in Collective Volume 10 p. 289, Annual Volume 78 p. 169

SYNTHESIS OF β-LACTONES BY ALDOLIZATION OF KETONES WITH PHENYL ESTER ENOLATES: 3,3-DIMETHYL-1-OXASPIRO[3.5]NONAN-2-ONE
Submitted by: Christine Wedler and Hans Schick
Published in Collective Volume 10 p. 339, Annual Volume 75 p. 116

[1.1.1]PROPELLANE
Submitted by: Kathleen R. Mondanaro and William P. Dailey
Published in Collective Volume 10 p. 658, Annual Volume 75 p. 98

PHENYLTHIOACETYLENE
Submitted by: Plato A. Magriotis and John T. Brown
Published in Collective Volume 9 p. 656, Annual Volume 72 p. 252

SPIROANNELATION VIA ORGANOBIS(CUPRATES): 9,9-DIMETHYLSPIRO[4.5]DECAN-7-ONE
Submitted by: Paul A. Wender, Alan W. White, and Frank E. McDonald
Published in Collective Volume 9 p. 350, Annual Volume 70 p. 204

SYNTHESIS OF β-LACTONES AND ALKENES VIA THIOL ESTERS: (E)-2,3-DIMETHYL-3-DODECENE
Submitted by: Rick L. Danheiser, James S. Nowick, Janette H. Lee, Raymond F. Miller, and Alexandre H. Huboux
Published in Collective Volume 9 p. 293, Annual Volume 73 p. 61

(PHENYLTHIO)NITROMETHANE
Submitted by: Anthony G. M. Barrett, Dashyant Dhanak, Gregory G. Graboski, and Sven J. Taylor
Published in Collective Volume 8 p. 550, Annual Volume 68 p. 8

PHENYL VINYL SULFONE AND SULFOXIDE
Submitted by: Leo A. Paquette and Richard V. C. Carr
Published in Collective Volume 7 p. 453, Annual Volume 64 p. 157

ACYLOIN CONDENSATION BY THIAZOLIUM ION CATALYSIS: BUTYROIN
Submitted by: H. Stetter and H. Kuhlmann
Published in Collective Volume 7 p. 95, Annual Volume 62 p. 170

PREPARATION OF THIOL ESTERS: S-tert-BUTYL CYCLOHEXANECARBOTHIOATE AND S-tert-BUTYL 3α,7α,12α-TRIHYDROXY-5β-CHOLANE-24-THIOATE
Submitted by: Gary O. Spessard, Wan Kit Chan, and S. Masamune
Published in Collective Volume 7 p. 81, Annual Volume 61 p. 134

2-THIOPHENETHIOL
Submitted by: E. Jones and I. M. Moodie
Published in Collective Volume 6 p. 979, Annual Volume 50 p. 104

SULFIDE SYNTHESIS IN PREPARATION OF DIALKYL AND ALKYL ARYL SULFIDES: NEOPENTYL PHENYL SULFIDE
Submitted by: D. Landini and F. Rolla
Published in Collective Volume 6 p. 833, Annual Volume 58 p. 143

VINYL SULFIDES FROM THIOACETALS WITH COPPER(I) TRIFLUOROMETHANESULFONATE: (Z)-2-METHOXY-1-PHENYLTHIO-1,3-BUTADIENE
Submitted by: Theodore Cohen, Robert J. Ruffner, David W. Shull, Elaine R. Fogel, and J. R. Falck
Published in Collective Volume 6 p. 737, Annual Volume 59 p. 202

SECONDARY AND TERTIARY ALKYL KETONES FROM CARBOXYLIC ACID CHLORIDES AND LITHIUM PHENYLTHIO(ALKYL)CUPRATE REAGENTS: tert-BUTYL PHENYL KETONE
Submitted by: Gary H. Posner and Charles E. Whitten
Published in Collective Volume 6 p. 248, Annual Volume 55 p. 122

VINYL TRIPHENYLPHOSPHONIUM BROMIDE
Submitted by: Edward E. Schweizer and Robert D. Bach
Published in Collective Volume 5 p. 1145, Annual Volume 48 p. 129

β-ISOVALEROLACTAM-N-SULFONYL CHLORIDE AND β-ISOVALEROLACTAM
Submitted by: Roderich Graf
Published in Collective Volume 5 p. 673, Annual Volume 46 p. 51

trans-4,4'-DIMETHOXYSTILBENE
Submitted by: J. W. A. Findlay and A. B. Turner
Published in Collective Volume 5 p. 428, Annual Volume 49 p. 53

1,2-BIS(n-BUTYLTHIO)BENZENE
Submitted by: Roger Adams, Walter Reifschneider, and Aldo Ferretti
Published in Collective Volume 5 p. 107, Annual Volume 42 p. 22

p-TOLUENESULFENYL CHLORIDE
Submitted by: Frederick Kurzer and J. Roy Powell
Published in Collective Volume 4 p. 934, Annual Volume 35 p. 99

1,5-NAPHTHALENEDITHIOL
Submitted by: P. D. Caesar
Published in Collective Volume 4 p. 695, Annual Volume 33 p. 47

DIPHENYL SULFIDE
Submitted by: W. W. Hartman, L. A. Smith, and J. B. Dickey
Published in Collective Volume 2 p. 242, Annual Volume 14 p. 36

THIOPHENOL
Submitted by: Roger Adams and C. S. Marvel
Published in Collective Volume 1 p. 504, Annual Volume 1 p. 71