Preps in which argon appears:
2-SUBSTITUTED-1,3-CYCLOHEXADIENES BY INTERMOLECULAR, METHYLENE-FREE TANDEM ENYNE METATHESIS
Submitted by: Amol A. Kulkarni and Steven T. Diver
Published in Collective Volume 11 p. 552,
Annual Volume 83 p. 200
TRIFLUOROMETHANESULFONIMIDE-CATALYZED (2 + 2)-CYCLOADDITION OF SILYL ENOL ETHERS WITH α,β-UNSATURATED ESTERS: 1-(tert-BUTYLDIMETHYLSILOXY)-8-(METHOXYCARBONYL)-6-METHYLBICYCLO[4.2.0]OCTANE
Submitted by: Kiyosei Takasu, Takayuki Ishii, Kazato Inanaga, and Masataka Ihara
Published in Collective Volume 11 p. 481,
Annual Volume 83 p. 193
TRIFLUOROMETHYLATION AT THE α-POSITION OF α,β-UNSATURATED KETONES: 4-PHENYL-3-(TRIFLUOROMETHYL)BUTAN-2-ONE
Submitted by: Kazuyuki Sato, Masaaki Omote, Akira Ando, and Itsumaro Kumadaki
Published in Collective Volume 11 p. 336,
Annual Volume 83 p. 177
ALLYLBORONATION OF IMINES: 1-PHENYLHEX-5-EN-3-AMINE
Submitted by: Masaharu Sugiura, Keiichi Hirano, and Shu¯ Kobayashi
Published in Collective Volume 11 p. 691,
Annual Volume 83 p. 170
SYNTHESIS OF (+)-(1R,2S,9S)-11-METHYL-7,11-DIAZATRICYCLO[7.3.1.02,7]TRIDECANE, A (+)-SPARTEINE SURROGATE
Submitted by: Amanda J. Dixon, Matthew J. McGrath, and Peter O'Brien
Published in Collective Volume 11 p. 25,
Annual Volume 83 p. 141
COPPER-CATALYZED ELECTROPHILIC AMINATION OF DIORGANOZINC REAGENTS: 4-PHENYLMORPHOLINE
Submitted by: Ashley M. Berman and Jeffrey S. Johnson
Published in Collective Volume 11 p. 684,
Annual Volume 83 p. 31
PREPARATION OF ENANTIOMERICALLY ENRICHED (1S)-1-PHENYLPROPAN-1-AMINE HYDROCHLORIDE BY A CATALYTIC ADDITION OF DIORGANOZINC REAGENTS TO IMINES
Submitted by: Jean-Nicolas Desrosiers, Alexandre Côté, Alessandro A. Boezio, and André B. Charette
Published in Collective Volume 11 p. 749,
Annual Volume 83 p. 5
PREPARATION OF ENANTIOMERICALLY PURE (R,R)-BozPHOS
Submitted by: Alexandre Côté, Jean-Nicolas Desrosiers, Alessandro A. Boezio, and André B. Charette
Published in Collective Volume 11 p. 982,
Annual Volume 83 p. 1
CATALYTIC REDUCTION OF AMIDES TO AMINES WITH HYDROSILANES USING A TRIRUTHENIUM CARBONYL CLUSTER AS THE CATALYST
Submitted by: Yukihiro Motoyama, Chikara Itonaga, Toshiki Ishida, Mikihiro Takasaki, and Hideo Nagashima
Published in Collective Volume 11 p. 1,
Annual Volume 82 p. 188
(RS)-(+)-2-METHYL-2-PROPANESULFINAMIDE
Submitted by: Daniel J. Weix and Jonathan A. Ellman
Published in Collective Volume 11 p. 770,
Annual Volume 82 p. 157
PREPARATION OF [1-(METHOXYMETHYLCARBAMOYL)ETHYL] PHOSPHONIC ACID BIS-(2,2,2-TRIFLUOROETHYL) ESTER: A USEFUL INTERMEDIATE IN THE SYNTHESIS OF Z-UNSATURATED N-METHOXY-N-METHYLAMIDES
Submitted by: Amos B. Smith, III, Jason J. Beiger, Akin H. Davulcu, and Jason M. Cox
Published in Collective Volume 11 p. 992,
Annual Volume 82 p. 147
PREPARATION OF (TRIPHENYLPHOSPHORANYLIDENE)-KETENE FROM (METHOXYCARBONYLMETHYLENE)-TRIPHENYLPHOSPHORANE
Submitted by: Rainer Schobert
Published in Collective Volume 11 p. 986,
Annual Volume 82 p. 140
(R)-(+)-3,4-DIMETHYLCYCLOHEX-2-EN-1-ONE
Submitted by: James D. White, Uwe M. Grether, and Chang-Sun Lee
Published in Collective Volume 11 p. 100,
Annual Volume 82 p. 108
1-(TERT-BUTYLIMINO-METHYL)-1,3-DIMETHYL-UREA HYDROCHLORIDE
Submitted by: David D. Díaz, Amy S. Ripka, and M. G. Finn
Published in Collective Volume 11 p. 782,
Annual Volume 82 p. 59
IRIDIUM-CATALYZED SYNTHESIS OF VINYL ETHERS FROM ALCOHOLS AND VINYL ACETATE
Submitted by: Tomotaka Hirabayashi, Satoshi Sakaguchi, and Yasutaka Ishii
Published in Collective Volume 11 p. 631,
Annual Volume 82 p. 55
PREPARATION OF (S,S)-1,2-BIS-(tert-BUTYLMETHYLPHOSPHINO)ETHANE ((S,S)-t-Bu-BISP*) AS A RHODIUM COMPLEX
Submitted by: Karen V. L. Crépy and Tsuneo Imamoto
Published in Collective Volume 11 p. 1020,
Annual Volume 82 p. 22
PHENYLSULFENYLATION OF NONACTIVATED δ-CARBON ATOM BY PHOTOLYSIS OF ALKYL BENZENESULFENATES: PREPARATION OF 2-PHENYLTHIO-5-HEPTANOL
Submitted by: Goran Petrovic, Radomir N. Saicic, and Živorad Cekovic
Published in Collective Volume 11 p. 121,
Annual Volume 81 p. 244
GENERATION OF NONRACEMIC 2-(t-BUTYLDIMETHYLSILYLOXY)-3-BUTYNYLLITHIUM FROM (S)-ETHYL LACTATE:
Submitted by: James A. Marshall, Mathew M. Yanik, Nicholas D. Adams, Keith C. Ellis, and Harry R. Chobanian
Published in Collective Volume 11 p. 615,
Annual Volume 81 p. 157
GENERATION AND CYCLIZATION OF 5-HEXENYLLITHIUM: 2-CYCLOPENTYLACETOPHENONE
Submitted by: William F. Bailey, Matthew R. Luderer, Michael J. Mealy, and Eric R. Punzalan
Published in Collective Volume 11 p. 433,
Annual Volume 81 p. 121
SYNTHESIS OF N-(tert-BUTOXYCARBONYL)-β-IODOALANINE METHYL ESTER: A USEFUL BUILDING BLOCK IN THE SYNTHESIS OF NONNATURAL α-AMINO ACIDS VIA PALLADIUM CATALYZED CROSS COUPLING REACTIONS
Submitted by: Richard F. W. Jackson and Manuel Perez-Gonzalez
Published in Collective Volume 11 p. 384,
Annual Volume 81 p. 77
HECK REACTIONS OF ARYL CHLORIDES CATALYZED BY PALLADIUM/TRI-tert-BUTYLPHOSPHINE: (E)-2-METHYL-3-PHENYLACRYLIC ACID BUTYL ESTER AND (E)-4-(2-PHENYLETHENYL)BENZONITRILE
Submitted by: Adam F. Littke and Gregory C. Fu
Published in Collective Volume 11 p. 372,
Annual Volume 81 p. 63
PLATINUM CATALYZED HYDROSILYLATION AND PALLADIUM CATALYZED CROSS-COUPLING: ONE-POT HYDROARYLATION OF 1-HEPTYNE TO (E)-1-(1-HEPTENYL)-4-METHOXYBENZENE
Submitted by: Scott E. Denmark and Zhigang Wang
Published in Collective Volume 11 p. 367,
Annual Volume 81 p. 54
TETRABENZYL PYROPHOSPHATE
Submitted by: Todd D. Nelson, Jonathan D. Rosen, M. Bhupathy, James McNamara, Michael J. Sowa, Chad Rush, and Louis S. Crocker
Published in Collective Volume 11 p. 1001,
Annual Volume 80 p. 219
PREPARATION OF α-ACETOXY ETHERS BY THE REDUCTIVE ACETYLATION OF ESTERS: endo-1-BORNYLOXYETHYL ACETATE
Submitted by: David J. Kopecky and Scott D. Rychnovsky
Published in Collective Volume 11 p. 52,
Annual Volume 80 p. 177
GENERATION AND [2+2] CYCLOADDITIONS OF THIO-SUBSTITUTED KETENES: trans-1-(4-METHOXYPHENYL)-4-PHENYL-3-(PHENYLTHIO)AZETIDIN-2-ONE
Submitted by: Rick L. Danheiser, Iwao Okamoto, Michael D. Lawlor, and Thomas W. Lee
Published in Collective Volume 11 p. 920,
Annual Volume 80 p. 160
PREPARATION OF SUBSTITUTED PYRIDINES VIA REGIOCONTROLLED [4 + 2] CYCLOADDITIONS OF OXIMINOSULFONATES: METHYL 5-METHYLPYRIDINE-2-CARBOXYLATE
Submitted by: Rick L. Danheiser, Adam R. Renslo, David T. Amos, and Graham T. Wright
Published in Collective Volume 11 p. 911,
Annual Volume 80 p. 133
GENERATION OF AN ACETYLENE-TITANIUM ALKOXIDE COMPLEX: PREPARATION OF (Z)-1,2-DIDEUTERIO-1-(TRIMETHYLSILYL)-1-HEXENE
Submitted by: Hirokazu Urabe, Daisuke Suzuki, and Fumie Sato
Published in Collective Volume 11 p. 600,
Annual Volume 80 p. 120
THE CATALYTIC INTRAMOLECULAR PAUSON-KHAND REACTION: 2,3,3α,4-TETRAHYDRO-2-[(4-METHYLBENZENE) SULFONYL]CYCLOPENTA[C]PYRROL-5(1H)-ONE
Submitted by: Mittun C. Patel, Tom Livinghouse, and Brian L. Pagenkopf
Published in Collective Volume 11 p. 442,
Annual Volume 80 p. 93
SYNTHESIS OF INDOLES BY PALLADIUM-CATALYZED REDUCTIVE N-HETEROANNULATION OF 2-NITROSTYRENES: METHYL INDOLE-4-CARBOXYLATE
Submitted by: Björn C. Söderberg, James A. Shriver, and Jeffery M. Wallace
Published in Collective Volume 11 p. 903,
Annual Volume 80 p. 75
(4S)-4-(1-METHYLETHYL)-5,5-DIPHENYL-2-OXAZOLIDINONE
Submitted by: Meinrad Brenner, Luigi La Vecchia, Thomas Leutert, and Dieter Seebach
Published in Collective Volume 11 p. 896,
Annual Volume 80 p. 57
SYNTHESIS OF (R,R)-4,6-DIBENZOFURANDIYL-2,2'-BIS (4-PHENYLOXAZOLINE) (DBFOX/PH) – A NOVEL TRIDENTATE LIGAND
Submitted by: Ulrich Iserloh, Yoji Oderaotoshi, Shuji Kanemasa, and Dennis P. Curran
Published in Collective Volume 11 p. 888,
Annual Volume 80 p. 46
4-METHOXYCARBONYL-2-METHYL-1,3-OXAZOLE
Submitted by: James D. White, Christian L. Kranemann, and Punlop Kuntiyong
Published in Collective Volume 10 p. 488,
Annual Volume 79 p. 244
PREPARATION OF 1-[N-BENZYLOXYCARBONYL-(1S)-1-AMINO-2-OXOETHYL]-4-METHYL-2,6,7-TRIOXABICYCLO[2.2.2]OCTANE
Submitted by: Nicholas G. W. Rose, Mark A. Blaskovich, Ghotas Evindar, Scott Wilkinson, Yue Luo, Dan Fishlock, Chris Reid, and Gilles A. Lajoie
Published in Collective Volume 10 p. 73,
Annual Volume 79 p. 216
3-(4-BROMOBENZOYL)PROPANOIC ACID
Submitted by: Alexander J. Seed, Vaishali Sonpatki, and Mark R. Herbert
Published in Collective Volume 10 p. 125,
Annual Volume 79 p. 204
(3,4,5-TRIFLUOROPHENYL)BORONIC ACID-CATALYZED AMIDE FORMATION FROM CARBOXYLIC ACIDS AND AMINES: N-BENZYL-4-PHENYLBUTYRAMIDE
Submitted by: Kazuaki Ishihara, Suguru Ohara, and Hisashi Yamamoto
Published in Collective Volume 10 p. 80,
Annual Volume 79 p. 176
PHOTO-INDUCED RING EXPANSION OF 1-TRIISOPROPYLSILYLOXY-1-AZIDOCYCLOHEXANE: PREPARATION OF ε-CAPROLACTAM
Submitted by: Jade D. Nelson, Dilip P. Modi, and P. Andrew Evans
Published in Collective Volume 10 p. 207,
Annual Volume 79 p. 165
CATALYTIC ENANTIOSELECTIVE ADDITION OF DIALKYLZINCS TO ALDEHYDES USING (2S)-(−)-3-exo-(DIMETHYLAMINO)ISOBORNEOL [(2S)-DAIB]: (S)-1-PHENYL-1-PROPANOL
Submitted by: Masato Kitamura, Hiromasa Oka, Seiji Suga, and Ryoji Noyori
Published in Collective Volume 10 p. 635,
Annual Volume 79 p. 139
(2S)-(−)-3-exo-(DIMETHYLAMINO)ISOBORNEOL [(2S)-(−)-DAIB]
Submitted by: James D. White, Duncan J. Wardrop, and Kurt F. Sundermann
Published in Collective Volume 10 p. 305,
Annual Volume 79 p. 130
ASYMMETRIC SYNTHESIS OF (M)-2-HYDROXYMETHYL-1-(2-HYDROXY-4,6-DIMETHYLPHENYL)NAPHTHALENE VIA A CONFIGURATIONALLY UNSTABLE BIARYL LACTONE
Submitted by: Gerhard Bringmann, Matthias Breuning, Petra Henschel, and Jürgen Hinrichs
Published in Collective Volume 10 p. 448,
Annual Volume 79 p. 72
SYNTHESIS AND UTILIZATION OF INDIUM (I) IODIDE FOR IN SITU FORMATION OF ENANTIOENRICHED ALLENYLINDIUM REAGENTS AND THEIR ADDITION TO ALDEHYDES: (2R,3S,4S)-1-(tert-BUTYLDIPHENYLSILYLOXY)-2,4-DIMETHYL-5-HEXYN-3-OL
Submitted by: Brian A. Johns, Charsetta M. Grant, and James A. Marshall
Published in Collective Volume 10 p. 170,
Annual Volume 79 p. 59
ETHYL 3-(p-CYANOPHENYL)PROPIONATE FROM ETHYL 3-IODOPROPIONATE AND p-CYANOPHENYLZINC BROMIDE
Submitted by: Anne Eeg Jensen, Florian Kneisel, and Paul Knochel
Published in Collective Volume 10 p. 391,
Annual Volume 79 p. 35
MOLYBDENUM CARBONYL-CATALYZED ALKYNOL CYCLOISOMERIZATION: PREPARATION OF 2-PHENYL-2,3-DIHYDROFURAN
Submitted by: Frank E. McDonald and Brian H. White
Published in Collective Volume 10 p. 621,
Annual Volume 79 p. 27
SYNTHESIS OF TRIS(2-PERFLUOROHEXYLETHYL)TIN HYDRIDE: A HIGHLY FLUORINATED TIN HYDRIDE WITH ADVANTAGEOUS FEATURES OF EASY PURIFICATION
Submitted by: Aimee Crombie, Sun-Young Kim, Sabine Hadida, and Dennis P. Curran
Published in Collective Volume 10 p. 712,
Annual Volume 79 p. 1
TRIBUTYLSTANNANE (Bu3SnH)-CATALYZED BARTON-McCOMBIE DEOXYGENATION OF ALCOHOLS: 3-DEOXY-1,2:5,6-BIS-O-(1-METHYLETHYLIDENE)-α-D-RIBO-HEXOFURANOSE
Submitted by: Jordi Tormo and Gregory C. Fu
Published in Collective Volume 10 p. 240,
Annual Volume 78 p. 239
PREPARATION AND DIELS-ALDER REACTION OF A 2-AMIDO SUBSTITUTED FURAN: tert-BUTYL 3a-METHYL-5-OXO-2,3,3a,4,5,6-HEXAHYDROINDOLE-1-CARBOXYLATE
Submitted by: Albert Padwa, Michael A. Brodney, and Stephen M. Lynch
Published in Collective Volume 10 p. 188,
Annual Volume 78 p. 202
(+)-(1R,2S,3R)-TETRACARBONYL[(1-3η)-1-(PHENYLSULFONYL)- BUT-2-EN-1-YL]IRON(1+) TETRAFLUOROBORATE
Submitted by: D. Enders, B. Jandeleit, and S. von Berg
Published in Collective Volume 10 p. 672,
Annual Volume 78 p. 189
SYNTHESIS OF (−)-(E,S)-3-(BENZYLOXY)-1-BUTENYL PHENYL SULFONE VIA A HORNER-WADSWORTH-EMMONS REACTION OF (−)-(S)-2-(BENZYLOXY)PROPANAL
Submitted by: D. Enders, S. von Berg, and B. Jandeleit
Published in Collective Volume 10 p. 66,
Annual Volume 78 p. 177
(1'R)-(−)-2,4-O-ETHYLIDENE-D-ERYTHROSE AND ETHYL (E)-(−)-4,6-O-ETHYLIDENE-(4S,5R,1'R)-4,5,6-TRIHYDROXY-2-HEXENOATE
Submitted by: M. Fengler-Veith, O. Schwardt, U. Kautz, B. Krämer, and V. Jäger
Published in Collective Volume 10 p. 405,
Annual Volume 78 p. 123
4-HYDROXY[1-13C]BENZOIC ACID
Submitted by: Martin Lang, Susanne Lang-Fugmann, and Wolfgang Steglich
Published in Collective Volume 10 p. 432,
Annual Volume 78 p. 113
PREPARATION AND USE OF N,N'-DI-BOC-N''-TRIFLYLGUANIDINE
Submitted by: Tracy J. Baker, Mika Tomioka, and Murray Goodman
Published in Collective Volume 10 p. 266,
Annual Volume 78 p. 91
PALLADIUM-CATALYZED AMINATION OF ARYL HALIDES AND ARYL TRIFLATES: N-HEXYL-2-METHYL-4-METHOXYANILINE AND N-METHYL-N-(4-CHLOROPHENYL)ANILINE
Submitted by: John P. Wolfe and Stephen L. Buchwald
Published in Collective Volume 10 p. 423,
Annual Volume 78 p. 23
CATALYTIC ASYMMETRIC SYNTHESIS OF NITROALDOLS USING A LANTHANUM-LITHIUM-BINOL COMPLEX:
(2S,3S)-2-NITRO-5-PHENYL-1,3-PENTANEDIOL
Submitted by: Hiroaki Sasai, Shizue Watanabe, Takeyuki Suzuki, and Masakatsu Shibasaki
Published in Collective Volume 10 p. 571,
Annual Volume 78 p. 14
CYCLOPROPENE: A NEW SIMPLE SYNTHESIS AND ITS DIELS-ALDER REACTION WITH CYCLOPENTADIENE
Submitted by: Paul Binger, Petra Wedemann, and Udo H. Brinker
Published in Collective Volume 10 p. 231,
Annual Volume 77 p. 254
METHYL 2,3-O-(6,6'-OCTAHYDRO-6,6'-BI-2H-PYRAN-2,2'-DIYL)-α-D-GALACTOPYRANOSIDE
Submitted by: Steven V. Ley and Helen M.I. Osborn
Published in Collective Volume 10 p. 552,
Annual Volume 77 p. 212
β-MERCAPTOPROPIONITRILE (2-CYANOETHANETHIOL)
Submitted by: R. Eric Gerber, Carlos Hasbun, Larisa G. Dubenko, Mei Fong King, and Donald E. Bierer
Published in Collective Volume 10 p. 234,
Annual Volume 77 p. 186
SYNTHESIS OF 2'-DEOXYRIBONUCLEOSIDES: β-3',5'-DI-O-BENZOYLTHYMIDINE
Submitted by: Daniel R. Prudhomme, Minnie Park, Zhiwei Wang, Jason R. Buck, and Carmelo J. Rizzo
Published in Collective Volume 10 p. 246,
Annual Volume 77 p. 162
9-ETHYL-3,6-DIMETHYLCARBAZOLE (DMECZ)
Submitted by: Jason R. Buck, Minnie Park, Zhiwei Wang, Daniel R. Prudhomme, and Carmelo J. Rizzo
Published in Collective Volume 10 p. 396,
Annual Volume 77 p. 153
THE DESS-MARTIN PERIODINANE: 1,1,1-TRIACETOXY-1,1-DIHYDRO-1,2-BENZIODOXOL-3(1H)-ONE
Submitted by: Robert K. Boeckman, Pengcheng Shao, and Joseph J. Mullins
Published in Collective Volume 10 p. 696,
Annual Volume 77 p. 141
7α-ACETOXY-(1Hβ, 6Hβ)-BICYCLO[4.4.1]UNDECA-2,4,8-TRIENE VIA CHROMIUM-MEDIATED HIGHER ORDER CYCLOADDITION
Submitted by: James H. Rigby and Kevin R. Fales
Published in Collective Volume 10 p. 1,
Annual Volume 77 p. 121
SYNTHESIS OF (S,E)-1-(METHOXYMETHOXY)-1-TRIBUTYLSTANNYL-2-BUTENE
Submitted by: James A. Marshall, Albert W. Garofalo, and Kevin W. Hinkle
Published in Collective Volume 10 p. 496,
Annual Volume 77 p. 98
SULFINIMINES (THIOOXIMINE S-OXIDES): ASYMMETRIC SYNTHESIS OF METHYL (R)-(+)-β-PHENYLALANATE FROM (S)-(+)-N-(BENZYLIDENE)-p-TOLUENESULFINAMIDE
Submitted by: Dean L. Fanelli, Joanna M. Szewczyk, Yulian Zhang, G. Venkat Reddy, David M. Burns, and Franklin A. Davis
Published in Collective Volume 10 p. 47,
Annual Volume 77 p. 50
TRANSFORMATION OF PSEUDOEPHEDRINE AMIDES INTO HIGHLY ENANTIOMERICALLY ENRICHED ALDEHYDES, ALCOHOLS, AND KETONES
Submitted by: Andrew G. Myers, Bryant H. Yang, and Hou Chen
Published in Collective Volume 10 p. 509,
Annual Volume 77 p. 29
SYNTHESIS AND DIASTEREOSELECTIVE ALKYLATION OF PSEUDOEPHEDRINE AMIDES
Submitted by: Andrew G. Myers and Bryant H. Yang
Published in Collective Volume 10 p. 12,
Annual Volume 77 p. 22
PREPARATION OF (R,R)-1,2:4,5-DIEPOXYPENTANE
Submitted by: Scott D. Rychnovsky, George Griesgraber, and Jay P. Powers
Published in Collective Volume 10 p. 276,
Annual Volume 77 p. 1
VITAMIN D2 FROM ERGOSTEROL
Submitted by: Masami Okabe
Published in Collective Volume 10 p. 718,
Annual Volume 76 p. 275
ISOMERIZATION OF β-ALKYNYL ALLYLIC ALCOHOLS TO FURANS CATALYZED BY SILVER NITRATE ON SILICA GEL: 2-PENTYL-3-METHYL-5-HEPTYLFURAN
Submitted by: James A. Marshall and Clark A. Sehon
Published in Collective Volume 10 p. 599,
Annual Volume 76 p. 263
COPPER-CATALYZED CONJUGATE ADDITION OF FUNCTIONALIZED ORGANOZINC REAGENTS TO α,β-UNSATURATED KETONES: ETHYL 5-(3-OXOCYCLOHEXYL)PENTANOATE
Submitted by: B. H. Lipshutz, M. R. Wood, and R. Tirado
Published in Collective Volume 10 p. 411,
Annual Volume 76 p. 252
REGIOSELECTIVE MONOALKYLATION OF KETONES VIA THEIR MANGANESE ENOLATES: 2-BENZYL-6-METHYLCYCLOHEXANONE FROM 2-METHYLCYCLOHEXANONE
Submitted by: Gérard Cahiez, François Chau, and Bernard Blanchot
Published in Collective Volume 10 p. 59,
Annual Volume 76 p. 239
USE OFCERIUM(III) CHLORIDE IN THE REACTIONS OF CARBONYL COMPOUNDS WITH ORGANOLITHIUMS OR GRIGNARD REAGENTS FOR THE SUPPRESSION OF ABNORMAL REACTIONS:1-BUTYL-1,2,3,4-TETRAHYDRO-1-NAPHTHOL
Submitted by: Nobuhiro Takeda and Tsuneo Imamoto
Published in Collective Volume 10 p. 200,
Annual Volume 76 p. 228
(tert-BUTYLDIMETHYLSILYL)ALLENE
Submitted by: Andrew G. Myers and Bin Zheng
Published in Collective Volume 10 p. 165,
Annual Volume 76 p. 178
ETHYL 5-CHLORO-3-PHENYLINDOLE-2-CARBOXYLATE
Submitted by: Alois Fürstner, Achim Hupperts, and Günter Seidel
Published in Collective Volume 10 p. 382,
Annual Volume 76 p. 142
CONVERSION OF NITRILES INTO TERTIARY AMINES: N,N-DIMETHYLHOMOVERATRYLAMINE
Submitted by: Guilhem Rousselet, Patrice Capdevielle, and Michel Maumy
Published in Collective Volume 10 p. 327,
Annual Volume 76 p. 133
METHYL (S)-2-PHTHALIMIDO-4-OXOBUTANOATE
Submitted by: Patrick Meffre, Philippe Durand, and François Le Goffic
Published in Collective Volume 10 p. 562,
Annual Volume 76 p. 123
PREPARATION OF ENANTIOMERICALLY PURE α-N,N-DIBENZYLAMINO ALDEHYDES: S-2-(N,N-DIBENZYLAMINO)-3-PHENYLPROPANAL
Submitted by: Manfred T. Reetz, Mark W. Drewes, and Renate Schwickardi
Published in Collective Volume 10 p. 256,
Annual Volume 76 p. 110
SYNTHESIS OF CHIRAL NON-RACEMIC DIOLS FROM (S,S)-1,2,3,4-DIEPOXYBUTANE: (2S,3S)-DIHYDROXY-1,4-DIPHENYLBUTANE
Submitted by: Michael A. Robbins, Paul N. Devine, and Taeboem Oh
Published in Collective Volume 10 p. 297,
Annual Volume 76 p. 101
(2S,3S)-(+)-(3-PHENYLCYCLOPROPYL)METHANOL
Submitted by: André B. Charette and Hélène Lebel
Published in Collective Volume 10 p. 613,
Annual Volume 76 p. 86
ASYMMETRIC SYNTHESIS OF α-AMINO ACIDS BY THE ALKYLATION OF PSEUDOEPHEDRINE GLYCINAMIDE: L-ALLYLGLYCINE AND N-BOC-L-ALLYLGLYCINE
Submitted by: Andrew G. Myers and James L. Gleason
Published in Collective Volume 10 p. 12,
Annual Volume 76 p. 57
1S-(−)-1,3-DITHIANE 1-OXIDE
Submitted by: Philip C. Bulman Page, Jag P. Heer, Donald Bethell, Eric W. Collington, and David M. Andrews
Published in Collective Volume 10 p. 378,
Annual Volume 76 p. 37
(4R,5R)-2,2-DIMETHYL-α,α,α',α'-TETRA(NAPHTH-2-YL)-1,3-DIOXOLANE-4,5-DIMETHANOL FROM DIMETHYL TARTRATE AND 2-NAPHTHYL-MAGNESIUM BROMIDE
Submitted by: Albert K. Beck, Peter Gysi, Luigi La Vecchia, and Dieter Seebach
Published in Collective Volume 10 p. 349,
Annual Volume 76 p. 12
USE OF 1,2,4,5-TETRABROMOBENZENE AS A 1,4-BENZADIYNE EQUIVALENT: anti- AND syn-1,4,5,8-TETRAHYDROANTHRACENE 1,4:5,8-DIEPOXIDES
Submitted by: Khalil Shahlai, Samuel Osafo Acquaah, and Harold Hart
Published in Collective Volume 10 p. 678,
Annual Volume 75 p. 201
6,7-DIHYDROCYCLOPENTA-1,3-DIOXIN-5(4H)-ONE
Submitted by: Kwunmin Chen, Christopher S. Brook, and Amos B. Smith, III
Published in Collective Volume 10 p. 293,
Annual Volume 75 p. 189
(1'S,2'S)-METHYL-3O,4O-(1',2'-DIMETHOXYCYCLOHEXANE-1',2'-DIYL)-α-D-MANNOPYRANOSIDE
Submitted by: Steven V. Ley, Helen M. I. Osborn, Henning W. M. Priepke, and Stuart L. Warriner
Published in Collective Volume 10 p. 523,
Annual Volume 75 p. 170
2-TRIMETHYLSILYLETHANESULFONYL CHLORIDE (SES-Cl)
Submitted by: Steven M. Weinreb, Charles E. Chase, Peter Wipf, and Srikanth Venkatraman
Published in Collective Volume 10 p. 707,
Annual Volume 75 p. 161
WITTIG OLEFINATION OF PERFLUOROALKYL CARBOXYLIC ESTERS; SYNTHESIS OF 1,1,1-TRIFLUORO-2-ETHOXY-5-PHENYLPENT-2-ENE AND 1-PERFLUOROALKYL EPOXY ETHERS: 1,1,1-TRIFLUORO-2-ETHOXY-2,3-EPOXY-5-PHENYLPENTANE
Submitted by: Jean-Pierre Bégué, Danièle Bonnet-Delpon, and Andrei Kornilov
Published in Collective Volume 10 p. 703,
Annual Volume 75 p. 153
EFFICIENT SYNTHESIS OF BROMIDES FROM CARBOXYLIC ACIDS CONTAINING A SENSITIVE FUNCTIONAL GROUP: DEC-9-ENYL BROMIDE FROM 10-UNDECENOIC ACID
Submitted by: Derek H. R. Barton, John MacKinnon, Roland N. Perchet, and Chi-Lam (Ivan) Tse
Published in Collective Volume 10 p. 237,
Annual Volume 75 p. 124
SYNTHESIS OF β-LACTONES BY ALDOLIZATION OF KETONES WITH PHENYL ESTER ENOLATES: 3,3-DIMETHYL-1-OXASPIRO[3.5]NONAN-2-ONE
Submitted by: Christine Wedler and Hans Schick
Published in Collective Volume 10 p. 339,
Annual Volume 75 p. 116
[1.1.1]PROPELLANE
Submitted by: Kathleen R. Mondanaro and William P. Dailey
Published in Collective Volume 10 p. 658,
Annual Volume 75 p. 98
2-(4-METHOXYPHENYL)-2-CYCLOHEXEN-1-ONE: PREPARATION OF 2-IODO-2-CYCLOHEXEN-1-ONE AND SUZUKI COUPLING WITH 4-METHOXYPHENYLBORONIC ACID
Submitted by: Frederic S. Ruel, Matthew P. Braun, and Carl R. Johnson
Published in Collective Volume 10 p. 467,
Annual Volume 75 p. 69
ACCELERATED SUZUKI COUPLING VIA A LIGANDLESS PALLADIUM CATALYST: 4-METHOXY-2'-METHYLBIPHENYL
Submitted by: Felix E. Goodson, Thomas I. Wallow, and Bruce M. Novak
Published in Collective Volume 10 p. 501,
Annual Volume 75 p. 61
(4R,5S)-4,5-DIPHENYL-3-VINYL-2-OXAZOLIDINONE
Submitted by: T. Akiba, O. Tamura, and S. Terashima
Published in Collective Volume 10 p. 374,
Annual Volume 75 p. 45
ASYMMETRIC SYNTHESIS OF DIETHYL (R)-(−)-(1-AMINO-3-METHYLBUTYL)PHOSPHONATE
Submitted by: Amos B. Smith, III, Kraig M. Yager, Barton W. Phillips, and Carol M. Taylor
Published in Collective Volume 10 p. 282,
Annual Volume 75 p. 19
TRIS(TRIMETHYLSILYL)SILANE
Submitted by: Joachim Dickhaut and Bernd Giese
Published in Collective Volume 9 p. 738,
Annual Volume 70 p. 164
A WATER-SOLUBLE TIN HYDRIDE: TRIS[3-(2-METHOXYETHOXY)PROPYL]STANNANE
Submitted by: James Light and Ronald Breslow
Published in Collective Volume 9 p. 733,
Annual Volume 72 p. 199
1,2,3-TRIPHENYLCYCLOPROPENIUM BROMIDE
Submitted by: Ruo Xu and Ronald Breslow
Published in Collective Volume 9 p. 730,
Annual Volume 74 p. 72
CHIRAL (ACYLOXY)BORANE COMPLEX-CATALYZED ASYMMETRIC DIELS-ALDER REACTION: (1R)-1,3,4-TRIMETHYL-3-CYCLOHEXENE-1-CARBOXALDEHYDE
Submitted by: Kyoji Furuta, Qing-zhi Gao, and Hisashi Yamamoto
Published in Collective Volume 9 p. 722,
Annual Volume 72 p. 86
A HYDROXYMETHYL ANION EQUIVALENT: TRIBUTYL[(METHOXYMETHOXY)METHYL]STANNANE
Submitted by: Rick L. Danheiser, Karen R. Romines, Hiroo Koyama, Stephen K. Gee, Carl R. Johnson, and John R. Medich
Published in Collective Volume 9 p. 704,
Annual Volume 71 p. 133
(S)-TETRAHYDRO-1-METHYL-3,3-DIPHENYL-1H,3H-PYRROLO-[1,2-c][1,3,2]OXAZABOROLE-BORANE COMPLEX
Submitted by: Lyndon C. Xavier, Julie J. Mohan, David J. Mathre, Andrew S. Thompson, James D. Carroll, Edward G. Corley, and Richard Desmond
Published in Collective Volume 9 p. 676,
Annual Volume 74 p. 50
PREPARATION OF POLYQUINANES BY DOUBLE ADDITION OF VINYL ANIONS TO SQUARATE ESTERS: 4,5,6,6a-TETRAHYDRO-3a-HYDROXY-2,3-DIISOPROPOXY-4,6a-DIMETHYL-1(3aH)-PENTALENONE
Submitted by: Tina Morwick and Leo A. Paquette
Published in Collective Volume 9 p. 670,
Annual Volume 74 p. 169
PHENYLTHIOACETYLENE
Submitted by: Plato A. Magriotis and John T. Brown
Published in Collective Volume 9 p. 656,
Annual Volume 72 p. 252
CONJUGATE ADDITION OF A VINYLZIRCONIUM REAGENT: 3-(1-OCTEN-1-YL)CYCLOPENTANONE
Submitted by: Ruen Chu Sun, Masami Okabe, David L. Coffen, and Jeffrey Schwartz
Published in Collective Volume 9 p. 640,
Annual Volume 71 p. 83
SYNTHESIS OF (S)-2-METHYLPROLINE: A GENERAL METHOD FOR THE PREPARATION OF α-BRANCHED AMINO ACIDS
Submitted by: A. K. Beck, S. Blank, K. Job, D. Seebach, and Th. Sommerfeld
Published in Collective Volume 9 p. 626,
Annual Volume 72 p. 62
INDOLE-2-ACETIC ACID METHYL ESTERS: METHYL 5-METHOXYINDOLE-2-ACETATE
Submitted by: Sandeep P. Modi, R. Christopher Oglesby, and Sydney Archer
Published in Collective Volume 9 p. 601,
Annual Volume 72 p. 125
ASYMMETRIC CATALYTIC GLYOXYLATE-ENE REACTION: METHYL (2R)-2-HYDROXY-4-PHENYL-4-PENTENOATE
Submitted by: Koichi Mikami, Masahiro Terada, Satoshi Narisawa, and Takeshi Nakai
Published in Collective Volume 9 p. 596,
Annual Volume 71 p. 14
ASYMMETRIC HYDROGENATION OF 3-OXO CARBOXYLATES USING BINAP-RUTHENIUM COMPLEXES: (R)-(−)-METHYL 3-HYDROXYBUTANOATE
Submitted by: Masato Kitamura, Makoto Tokunaga, Takeshi Ohkuma, and Ryoji Noyori
Published in Collective Volume 9 p. 589,
Annual Volume 71 p. 1
STEREOSELECTIVE ALKENE SYNTHESIS via 1-CHLORO-1-[(DIMETHYL)PHENYLSILYL]ALKANES AND α-(DIMETHYL)PHENYLSILYL KETONES: 6-METHYL-6-DODECENE
Submitted by: Anthony G. M. Barrett, John A. Flygare, Jason M. Hill, and Eli M. Wallace
Published in Collective Volume 9 p. 580,
Annual Volume 73 p. 50
(E,Z)-1-METHOXY-2-METHYL-3-(TRIMETHYLSILOXY)-1,3-PENTADIENE
Submitted by: David C. Myles and Mathew H. Bigham
Published in Collective Volume 9 p. 548,
Annual Volume 70 p. 231
REGIO- AND STEREOSELECTIVE INTRAMOLECULAR HYDROSILYLATION OF α-HYDROXY ENOL ETHERS: 2,3-syn-2-METHOXYMETHOXY-1,3-NONANEDIOL
Submitted by: Kohei Tamao, Yoshiki Nakagawa, and Yoshihiko Ito
Published in Collective Volume 9 p. 539,
Annual Volume 73 p. 94
ACETYLENIC ETHERS FROM ALCOHOLS AND THEIR REDUCTION TO Z- AND E-ENOL ETHERS: PREPARATION OF 1-MENTHOXY-1-BUTYNE FROM MENTHOL AND CONVERSION TO (Z)- AND (E)-1-MENTHOXY-1-BUTENE
Submitted by: Nina Kann, Vania Bernardes, and Andrew E. Greene
Published in Collective Volume 9 p. 533,
Annual Volume 74 p. 13
4-KETOUNDECANOIC ACID
Submitted by: M. A. Tschantz, L. E. Burgess, and A. I. Meyers
Published in Collective Volume 9 p. 530,
Annual Volume 73 p. 215
TITANIUM-MEDIATED ADDITION OF SILYL DIENOL ETHERS TO ELECTROPHILIC GLYCINE: 4-KETOPIPECOLIC ACID HYDROCHLORIDE
Submitted by: Clarisse Mühlemann, Peter Hartmann, and Jean-Pierre Obrecht
Published in Collective Volume 9 p. 526,
Annual Volume 71 p. 200
IODOLACTAMIZATION: 8-exo-IODO-2-AZABICYCLO[3.3.0]OCTAN-3-ONE
Submitted by: Spencer Knapp and Frank S. Gibson
Published in Collective Volume 9 p. 516,
Annual Volume 70 p. 101
1,2-ADDITION OF A FUNCTIONALIZED ZINC-COPPER ORGANOMETALLIC [RCu(CN)ZnI] TO AN α,β-UNSATURATED ALDEHYDE: (E)-2-(4-HYDROXY-6-PHENYL-5-HEXENYL)-1H-ISOINDOLE-1,3(2H)-DIONE
Submitted by: Ming Chang P. Yeh, Huai Gu Chen, and Paul Knochel
Published in Collective Volume 9 p. 502,
Annual Volume 70 p. 195
PREPARATION AND USE OF (METHOXYMETHOXY)METHYLLITHIUM: 1-(HYDROXYMETHYL)CYCLOHEPTANOL
Submitted by: Carl R. Johnson, John R. Medich, Rick L. Danheiser, Karen R. Romines, Hiroo Koyama, and Stephen K. Gee
Published in Collective Volume 9 p. 493,
Annual Volume 71 p. 140
ENANTIOSELECTIVE HYDROLYSIS OF cis-3,5-DIACETOXYCYCLOPENTENE: (1R,4S)-(+)-4-HYDROXY-2-CYCLOPENTENYL ACETATE
Submitted by: Donald R. Deardorff, Colin Q. Windham, and Chris L. Craney
Published in Collective Volume 9 p. 487,
Annual Volume 73 p. 25
ALKYNYL(PHENYL)IODONIUM TOSYLATES: PREPARATION AND STEREOSPECIFIC COUPLING WITH VINYLCOPPER REAGENTS. FORMATION OF CONJUGATED ENYNES. 1-HEXYNYL(PHENYL)IODONIUM TOSYLATE AND (E)-5-PHENYLDODEC-5-EN-7-YNE
Submitted by: Peter J. Stang and Tsugio Kitamura
Published in Collective Volume 9 p. 477,
Annual Volume 70 p. 215
PREPARATION AND REACTIONS OF ALKENYLCHROMIUM REAGENTS: 2-HEXYL-5-PHENYL-1-PENTEN-3-OL
Submitted by: Kazuhiko Takai, Koichi Sakogawa, Yasutaka Kataoka, Koichiro Oshima, and Kiitiro Utimoto
Published in Collective Volume 9 p. 472,
Annual Volume 72 p. 180
S-(−)-5-HEPTYL-2-PYRROLIDINONE. CHIRAL BICYCLIC LACTAMS AS TEMPLATES FOR PYRROLIDINES AND PYRROLIDINONES
Submitted by: M. A. Tschantz, L. E. Burgess, and A. I. Meyers
Published in Collective Volume 9 p. 457,
Annual Volume 73 p. 221
REACTION OF SULFOXIDES WITH DIETHYLAMINOSULFUR TRIFLUORIDE: FLUOROMETHYL PHENYL SULFONE, A REAGENT FOR THE SYNTHESIS OF FLUOROALKENES
Submitted by: James R. McCarthy, Donald P. Matthews, and John P. Paolini
Published in Collective Volume 9 p. 446,
Annual Volume 72 p. 209
ETHYL 3-OXO-4-PENTENOATE (NAZAROV'S REAGENT)
Submitted by: R. Zibuck and J. Streiber
Published in Collective Volume 9 p. 432,
Annual Volume 71 p. 236
SYNTHESIS OF FURANS VIA RHODIUM(II) ACETATE-CATALYZED REACTION OF ACETYLENES WITH α-DIAZOCARBONYLS: ETHYL 2-METHYL-5-PHENYL-3-FURANCARBOXYLATE
Submitted by: Huw M. L. Davies, William R. Cantrell, Jr, Karen R. Romines, and Jonathan S. Baum
Published in Collective Volume 9 p. 422,
Annual Volume 70 p. 93
REGIOSELECTIVE SYNTHESIS OF 3-SUBSTITUTED INDOLES: 3-ETHYLINDOLE
Submitted by: Mercedes Amat, Sabine Hadida, Swargam Sathyanarayana, and Joan Bosch
Published in Collective Volume 9 p. 417,
Annual Volume 74 p. 248
CONVERSION OF METHYL KETONES INTO TERMINAL ACETYLENES: ETHYNYLFERROCENE
Submitted by: Johann Polin and Herwig Schottenberger
Published in Collective Volume 9 p. 411,
Annual Volume 73 p. 262
(R)-(+)-2-(DIPHENYLHYDROXYMETHYL)PYRROLIDINE
Submitted by: Nikola A. Nikolic and Peter Beak
Published in Collective Volume 9 p. 391,
Annual Volume 74 p. 23
(1R,2R)-(+)- AND (1S,2S)-(−)- 1,2-DIPHENYL-1,2-ETHYLENEDIAMINE
Submitted by: S. Pikul and E. J. Corey
Published in Collective Volume 9 p. 387,
Annual Volume 71 p. 22
REARRANGEMENT OF trans-STILBENE OXIDE TO DIPHENYLACETALDEHYDE WITH CATALYTIC METHYLALUMINUM BIS(4-BROMO-2,6-DI-tert-BUTYLPHENOXIDE)
Submitted by: Takashi Ooi, Keiji Maruoka, and Hisashi Yamamoto
Published in Collective Volume 9 p. 356,
Annual Volume 72 p. 95
MANGANESE-COPPER-CATALYZED CONJUGATE ADDITION OF ORGANOMAGNESIUM REAGENTS TO α,β-ETHYLENIC KETONES: 2-(1,1-DIMETHYLPENTYL)-5-METHYL-CYCLOHEXANONE FROM PULEGONE
Submitted by: S. Marquais, M. Alami, and G. Cahiez
Published in Collective Volume 9 p. 328,
Annual Volume 72 p. 135
REGIO- AND STEREOSELECTIVE CARBOXYLATION OF ALLYLIC BARIUM REAGENTS: (E)-4,8-DIMETHYL-3,7-NONADIENOIC ACID
Submitted by: Akira Yanagisawa, Katsutaka Yasue, and Hisashi Yamamoto
Published in Collective Volume 9 p. 317,
Annual Volume 74 p. 178
DIALKYL MESOXALATES BY OZONOLYSIS OF DIALKYL BENZALMALONATES: DIMETHYL MESOXALATE
Submitted by: Lutz F. Tietze and Matthias Bratz
Published in Collective Volume 9 p. 314,
Annual Volume 71 p. 214
DIASTEREOSELECTIVE FORMATION OF trans-1,2-DISUBSTITUTED CYCLOHEXANES FROM ALKYLIDENEMALONATES BY AN INTRAMOLECULAR ENE REACTION: DIMETHYL (1'R,2'R,5'R)-2-(2'-ISOPROPENYL-5'-METHYLCYCLOHEX-1'-YL)-PROPANE-1,3-DIOATE
Submitted by: L. F. Tietze and U. Beifuss
Published in Collective Volume 9 p. 310,
Annual Volume 71 p. 167
1,3-DIOLS FROM LITHIUM β-LITHIOALKOXIDES GENERATED BY THE REDUCTIVE LITHIATION OF EPOXIDES: 2,5-DIMETHYL-2,4-HEXANEDIOL
Submitted by: Boguslaw Mudryk and Theodore Cohen
Published in Collective Volume 9 p. 306,
Annual Volume 72 p. 173
1,1,-DIMETHYLETHYL (S)- OR (R)-4-FORMYL-2,2-DIMETHYL-3-OXAZOLIDINECARBOXYLATE: A USEFUL SERINAL DERIVATIVE
Submitted by: Philip Garner and Jung Min Park
Published in Collective Volume 9 p. 300,
Annual Volume 70 p. 18
3-[(1S)-1,2-DIHYDROXYETHYL]-1,5-DIHYDRO-3H-2,4-BENZODIOXEPINE
Submitted by: Ryu Oi and K. Barry Sharpless
Published in Collective Volume 9 p. 251,
Annual Volume 73 p. 1
DIETHYL 1-PROPYL-2-OXOETHYLPHOSPHONATE
Submitted by: Philippe Savignac and Carl Patois
Published in Collective Volume 9 p. 239,
Annual Volume 72 p. 241
CONVERSION OF AMINES TO PHOSPHO ESTERS: DECYL DIETHYL PHOSPHATE
Submitted by: Nick Nikolaides, Ioanna Schipor, and Bruce Ganem
Published in Collective Volume 9 p. 194,
Annual Volume 72 p. 246
BENZOANNELATION OF KETONES: 3,4-CYCLODODECENO-1-METHYLBENZENE
Submitted by: Marcus A. Tius and G. S. Kamali Kannangara
Published in Collective Volume 9 p. 180,
Annual Volume 71 p. 158
ASYMMETRIC HYDROGENATION OF ALLYLIC ALCOHOLS USING BINAP-RUTHENIUM COMPLEXES: (S)-(−)-CITRONELLOL
Submitted by: Hidemasa Takaya, Tetsuo Ohta, Shin-ichi Inoue, Makoto Tokunaga, Masato Kitamura, and Ryoji Noyori
Published in Collective Volume 9 p. 169,
Annual Volume 72 p. 74
PYRIDINE-DERIVED TRIFLATING REAGENTS: N-(2-PYRIDYL)-TRIFLIMIDE AND N-(5-CHLORO-2-PYRIDYL)TRIFLIMIDE
Submitted by: Daniel L. Comins, Ali Dehghani, Christopher J. Foti, and Sajan P. Joseph
Published in Collective Volume 9 p. 165,
Annual Volume 74 p. 77
SCHWARTZ'S REAGENT
Submitted by: Stephen L. Buchwald, Susan J. LaMaire, Ralph B. Nielsen, Brett T. Watson, and Susan M. King
Published in Collective Volume 9 p. 162,
Annual Volume 71 p. 77
PREPARATION AND REACTIONS OF 2-tert-BUTYL-1,1,3,3-TETRAMETHYLGUANIDINE: 2,2,6-TRIMETHYLCYCLOHEXEN-1-YL IODIDE
Submitted by: Derek H. R. Barton, Mi Chen, Joseph Cs. Jászberényi, and Dennis K. Taylor
Published in Collective Volume 9 p. 147,
Annual Volume 74 p. 101
ALLYLIC ALCOHOLS BY ALKENE TRANSFER FROM ZIRCONIUM TO ZINC: 1-[(tert-BUTYLDIPHENYLSILYL)OXY]-DEC-3-EN-5-OL
Submitted by: Peter Wipf and Wenjing Xu
Published in Collective Volume 9 p. 143,
Annual Volume 74 p. 205
3-(S)-[(tert-BUTYLDIPHENYLSILYL)OXY]-2-BUTANONE
Submitted by: Larry E. Overman and Gilbert M. Rishton
Published in Collective Volume 9 p. 139,
Annual Volume 71 p. 56
SYNTHESIS OF 7-SUBSTITUTED INDOLINES via DIRECTED LITHIATION OF 1-(tert-BUTOXYCARBONYL)INDOLINE: 7-INDOLINECARBOXALDEHYDE
Submitted by: Masatomo Iwao and Tsukasa Kuraishi
Published in Collective Volume 9 p. 124,
Annual Volume 73 p. 85
SYNTHESIS OF FUNCTIONALIZED ENYNES BY PALLADIUM/COPPER-CATALYZED COUPLING REACTIONS OF ACETYLENES WITH (Z)-2,3-DIBROMOPROPENOIC ACID ETHYL ESTER: (Z)-2-BROMO-5-(TRIMETHYLSILYL)-2-PENTEN-4-YNOIC ACID ETHYL ESTER
Submitted by: Andrew G. Myers and Peter S. Dragovich
Published in Collective Volume 9 p. 117,
Annual Volume 72 p. 104
BIS(TRIMETHYLSILYL) PEROXIDE (BTMSPO)
Submitted by: P. Dembech, A. Ricci, G. Seconi, and M. Taddei
Published in Collective Volume 9 p. 91,
Annual Volume 74 p. 84
ENANTIOSELECTIVE, CATALYTIC DIELS-ALDER REACTION: (1S-endo)-3-(BICYCLO[2.2.1]HEPT-5-EN-2-YLCARBONYL)-2-OXAZOLIDINONE
Submitted by: S. Pikul and E. J. Corey
Published in Collective Volume 9 p. 67,
Annual Volume 71 p. 30
SYNTHESIS OF N-PROTECTED α-AMINO ACIDS FROM N-(BENZYLOXYCARBONYL)-L-SERINE VIA ITS β-LACTONE: Nα-(BENZYLOXYCARBONYL)-β-(PYRAZOL-1-YL)-L-ALANINE
Submitted by: Sunil V. Pansare, Gregory Huyer, Lee D. Arnold, and John C. Vederas
Published in Collective Volume 9 p. 58,
Annual Volume 70 p. 1
DIASTEREOSELECTIVE HOMOLOGATION OF D-(R)-GLYCERALDEHYDE ACETONIDE USING 2-(TRIMETHYLSILYL)THIAZOLE: 2-O-BENZYL-3,4-ISOPROPYLIDENE-D-ERYTHROSE
Submitted by: Alessandro Dondoni and Pedro Merino
Published in Collective Volume 9 p. 52,
Annual Volume 72 p. 21
(E)-1-BENZYL-3-(1-IODOETHYLIDENE)PIPERIDINE: NUCLEOPHILE-PROMOTED ALKYNE-IMINIUM ION CYCLIZATIONS
Submitted by: H. Arnold, L. E. Overman, M. J. Sharp, and M. C. Witschel
Published in Collective Volume 9 p. 46,
Annual Volume 70 p. 111
(−)-2-O-BENZYL-L-GLYCERALDEHYDE AND ETHYL (R,E)-4-O-BENZYL-4,5-DIHYDROXY-2-PENTENOATE
Submitted by: B. Steuer, V. Wehner, A. Lieberknecht, and V. Jäger
Published in Collective Volume 9 p. 39,
Annual Volume 74 p. 1
4-BENZYL-10,19-DIETHYL-4,10,19-TRIAZA-1,7,13,16-TETRAOXACYCLOHENEICOSANE (TRIAZA-21-CROWN-7)
Submitted by: Krzysztof E. Krakowiak and Jerald S. Bradshaw
Published in Collective Volume 9 p. 34,
Annual Volume 70 p. 129
N-tert-BUTOXYCARBONYL-L-SERINE β-LACTONE AND (S)-3-AMINO-2-OXETANONE p-TOLUENESULFONIC ACID SALT
Submitted by: Sunil V. Pansare, Lee D. Arnold, and John C. Vederas
Published in Collective Volume 9 p. 24,
Annual Volume 70 p. 10
ENANTIOMERICALLY PURE β-AMINO ACIDS FROM 2-tert-BUTYL-1-CARBOMETHOXY-2,3-DIHYDRO-4(1H)-PYRIMIDINONE: (R)-3-AMINO-3-(p-METHOXYPHENYL)PROPIONIC ACID
Submitted by: F. J. Lakner, K. S. Chu, G. R. Negrete, and J. P. Konopelski
Published in Collective Volume 9 p. 17,
Annual Volume 73 p. 201
(3S,4S)-3-AMINO-1-(3,4-DIMETHOXYBENZYL)-4-[(R)-2,2-DIMETHYL-1,3-DIOXOLAN-4-YL]-2-AZETIDINONE
Submitted by: Christian Hubschwerlen and Jean-Luc Specklin
Published in Collective Volume 9 p. 13,
Annual Volume 72 p. 14
HIGHLY REACTIVE CALCIUM FOR THE PREPARATION OF ORGANOCALCIUM REAGENTS: 1-ADAMANTYL CALCIUM HALIDES AND THEIR ADDITION TO KETONES: 1-(1-ADAMANTYL)CYCLOHEXANOL
Submitted by: Reuben D. Rieke, Tse-Chong Wu, and Loretta I. Rieke
Published in Collective Volume 9 p. 9,
Annual Volume 72 p. 147
STEREOCONTROLLED PREPARATION OF 3-ACYLTETRAHYDROFURANS FROM ACID-PROMOTED REARRANGEMENTS OF ALLYLIC KETALS: (2S,3S)-3-ACETYL-8-CARBOETHOXY-2,3-DIMETHYL-1-OXA-8-AZASPIRO[4.5]DECANE
Submitted by: Larry E. Overman and Gilbert M. Rishton
Published in Collective Volume 9 p. 4,
Annual Volume 71 p. 63
TRIMETHYLSILYLDIAZOMETHANE
Submitted by: Takayuki Shioiri, Toyohiko Aoyama, and Shigehiro Mori
Published in Collective Volume 8 p. 612,
Annual Volume 68 p. 1
(−)-SALSOLIDINE
Submitted by: Albert I. Meyers, Michael Boes, and Daniel A. Dickman
Published in Collective Volume 8 p. 573,
Annual Volume 67 p. 60
2-PROPYL-1-AZACYCLOHEPTANE FROM CYCLOHEXANONE OXIME
Submitted by: Keiji Maruoka, Shuichi Nakai, and Hisashi Yamamoto
Published in Collective Volume 8 p. 568,
Annual Volume 66 p. 185
A GENERAL METHOD FOR THE PREPARATION OF 9-, 10-, AND 11-MEMBERED UNSATURATED MACROLIDES: SYNTHESIS OF 8-PROPIONYL-(E)-5-NONENOLIDE
Submitted by: Kevin S. Webb, Edward Asirvatham, and Gary H. Posner
Published in Collective Volume 8 p. 562,
Annual Volume 69 p. 188
(−)-α-PINENE BY ISOMERIZATION OF (−)-β-PINENE
Submitted by: Charles A. Brown and Prabhakav K. Jadhav
Published in Collective Volume 8 p. 553,
Annual Volume 65 p. 224
(±)-trans-2-(PHENYLSULFONYL)-3-PHENYLOXAZIRIDINE
Submitted by: Lal C. Vishwakarma, Orum D. Stringer, and Franklin A. Davis
Published in Collective Volume 8 p. 546,
Annual Volume 66 p. 203
α-UNSUBSTITUTED γ,δ-UNSATURATED ALDEHYDES BY CLAISEN REARRANGEMENT: 3-PHENYL-4-PENTENAL
Submitted by: Dennis E. Vogel and George H. Büchi
Published in Collective Volume 8 p. 536,
Annual Volume 66 p. 29
HYDROMAGNESIATION REACTION OF PROPARGYLIC ALCOHOLS: (E)-3-PENTYL-2-NONENE-1,4-DIOL FROM 2-OCTYN-1-OL
Submitted by: Fumie Sato and Yuichi Kobayashi
Published in Collective Volume 8 p. 507,
Annual Volume 69 p. 106
1,2,3,4,5-PENTAMETHYLCYCLOPENTADIENE
Submitted by: Richard S. Threlkel, John E. Bercaw, Paul F. Seidler, Jeffrey M. Stryker, and Robert G. Bergman
Published in Collective Volume 8 p. 505,
Annual Volume 65 p. 42
(1-OXO-2-PROPENYL)TRIMETHYLSILANE
Submitted by: Rick L. Danheiser, David M. Fink, Kazuo Okano, Yeun-Min Tsai, and Steven W. Szczepanski
Published in Collective Volume 8 p. 501,
Annual Volume 66 p. 14
3'-NITRO-1-PHENYLETHANOL BY ADDITION OF METHYLTRIISOPROPOXYTITANIUM TO m-NITROBENZALDEHYDE
Submitted by: René Imwinkelried and Dieter Seebach
Published in Collective Volume 8 p. 495,
Annual Volume 67 p. 180
INTRAMOLECULAR OXIDATIVE COUPLING OF A BISENOLATE: 4-METHYLTRICYCLO[2.2.2.03,5]OCTANE-2,6-DIONE
Submitted by: Marc-André Poupart, Gilbert Lassalle, and Leo A. Paquette
Published in Collective Volume 8 p. 467,
Annual Volume 68 p. 220
ENANTIOSELECTIVE OXIDATION OF A SULFIDE: (S)-(−)-METHYL p-TOLYL SULFOXIDE
Submitted by: S. H. Zhao, O. Samuel, and H. B. Kagan
Published in Collective Volume 8 p. 464,
Annual Volume 68 p. 49
PREPARATION AND INVERSE-ELECTRON-DEMAND DIELS–ALDER REACTION OF AN ELECTRON-DEFICIENT DIENE: METHYL 2-OXO-5,6,7,8-TETRAHYDRO-2H-1-BENZOPYRAN-3-CARBOXYLATE AND 6-METHOXY-7-METHOXYCARBONYL-1,2,3,4-TETRAHYDRONAPHTHALANE
Submitted by: Dale L. Boger and Michael D. Mullican
Published in Collective Volume 8 p. 444,
Annual Volume 65 p. 98
DIRECTED HOMOGENEOUS HYDROGENATION: METHYL anti-3-HYDROXY-2-METHYLPENTANOATE
Submitted by: John M. Brown, Phillip L. Evans, and Alun P. James
Published in Collective Volume 8 p. 420,
Annual Volume 68 p. 64
ASYMMETRIC SYNTHESES USING THE SAMP-/RAMP-HYDRAZONE METHOD: (S)-(+)-4-METHYL-3-HEPTANONE
Submitted by: Dieter Enders, Helmut Kipphardt, and Peter Fey
Published in Collective Volume 8 p. 403,
Annual Volume 65 p. 183
VINYL RADICAL CYCLIZATION VIA ADDITION OF TIN RADICALS TO TRIPLE BONDS: 3-METHYLENE-4-ISOPROPYL-1,1-CYCLOPENTANEDICARBOXYLIC ACID, DIMETHYL ESTER
Submitted by: Robert Mook, Jr and Philip Michael Sher
Published in Collective Volume 8 p. 381,
Annual Volume 66 p. 75
ALKOXYCARBONYLATION OF PROPARGYL CHLORIDE: METHYL 4-CHLORO-2-BUTYNOATE
Submitted by: M. Olomucki and J. Y. Le Gall
Published in Collective Volume 8 p. 371,
Annual Volume 65 p. 47
REGIOSELECTIVE SYNTHESIS OF TETRAHYDROPYRIDINES: 1-(4-METHOXYPHENYL)-1,2,5,6-TETRAHYDROPYRIDINE
Submitted by: Larry E. Overman, Chris J. Flann, and Thomas C. Malone
Published in Collective Volume 8 p. 358,
Annual Volume 68 p. 188
TRANSESTERIFICATION OF METHYL ESTERS OF AROMATIC AND α,β-UNSATURATED ACIDS WITH BULKY ALCOHOLS: (−)-MENTHYL CINNAMATE AND (−)-MENTHYL NICOTINATE
Submitted by: Otto Meth-Cohn
Published in Collective Volume 8 p. 350,
Annual Volume 68 p. 155
DIRECT NUCLEOPHILIC ACYLATION BY THE LOW-TEMPERATURE, IN SITU GENERATION OF ACYLLITHIUM REAGENTS; α-HYDROXY KETONES FROM KETONES: 3-HYDROXY-2,2,3-TRIMETHYLOCTAN-4-ONE FROM PINACOLONE
Submitted by: Richard Hui and Dietmar Seyferth
Published in Collective Volume 8 p. 343,
Annual Volume 69 p. 114
3-HYDROXY-3-METHYL-1-PHENYL-1-BUTANONE BY CROSSED ALDOL REACTION
Submitted by: Teruaki Mukaiyama and Koichi Narasaka
Published in Collective Volume 8 p. 323,
Annual Volume 65 p. 6
SELECTIVE CYCLOPROPANATION OF (S)-(−)-PERILLYL ALCOHOL: 1-HYDROXYMETHYL-4-(1-METHYLCYCLOPROPYL)-1-CYCLOHEXENE
Submitted by: Keiji Maruoka, Soichi Sakane, and Hisashi Yamamoto
Published in Collective Volume 8 p. 321,
Annual Volume 67 p. 176
A GENERAL SYNTHESIS OF CYCLOBUTANONES FROM OLEFINS AND TERTIARY AMIDES: 3-HEXYLCYCLOBUTANONE
Submitted by: C. Schmit, J. B. Falmagne, J. Escudero, H. Vanlierde, and L. Ghosez
Published in Collective Volume 8 p. 306,
Annual Volume 69 p. 199
DOMINO DIELS–ALDER REACTION: 3,3a,3b,4,6a,7a-HEXAHYDRO-3,4,7-METHENO-7H-CYCLOPENTA[a]PENTALENE-7,8-DICARBOXYLIC ACID
Submitted by: Richard T. Taylor, Michael W. Pelter, and Leo A. Paquette
Published in Collective Volume 8 p. 298,
Annual Volume 68 p. 198
PALLADIUM-CATALYZED SYNTHESIS OF CONJUGATED DIENES: (5Z,7E)-5,7-HEXADECADIENE
Submitted by: Ei-ichi Negishi, Tamotsu Takahashi, and Shigeru Baba
Published in Collective Volume 8 p. 295,
Annual Volume 66 p. 60
N-FLUOROPYRIDINIUM TRIFLATE: AN ELECTROPHILIC FLUORINATING AGENT
Submitted by: Teruo Umemoto, Kyoichi Tomita, and Kosuke Kawada
Published in Collective Volume 8 p. 286,
Annual Volume 69 p. 129
ENANTIOMERICALLY PURE ETHYL (R)- AND (S)- 2-FLUOROHEXANOATE BY ENZYME-CATALYZED KINETIC RESOLUTION
Submitted by: P. Kalaritis and R. W. Regenye
Published in Collective Volume 8 p. 258,
Annual Volume 69 p. 10
ASYMMETRIC SYNTHESIS OF 4,4-DIALKYLCYCLOHEXENONES FROM CHIRAL BICYCLIC LACTAMS: (R)-4-ETHYL-4-ALLYL-2-CYCLOHEXEN-1-ONE
Submitted by: Albert I. Meyers and Daniel Berney
Published in Collective Volume 8 p. 241,
Annual Volume 69 p. 55
PROPARGYLATION OF ALKYL HALIDES: (E)-6,10-DIMETHYL-5,9-UNDECADIEN-1-YNE AND (E)-7,11-DIMETHYL-6,10-DODECADIEN-2-YN-1-OL
Submitted by: John Hooz, Jorge Cabezas, Sergio Musmanni, and Jose Calzada
Published in Collective Volume 8 p. 226,
Annual Volume 69 p. 120
CYCLOPENTADIENE ANNULATION VIA THE SKATTEBØL REARRANGEMENT: (1R)-9,9-DIMETHYLTRICYCLO-[6.1.1.02,6]DECA-2,5-DIENE
Submitted by: Leo A. Paquette and Mark L. McLaughlin
Published in Collective Volume 8 p. 223,
Annual Volume p.
APROTIC DOUBLE MICHAEL ADDITION: 1,3-DIMETHYL-5-OXOBICYCLO[2.2.2]OCTANE-2-CARBOXYLIC ACID
Submitted by: Dietrich Spitzner and Anita Engler
Published in Collective Volume 8 p. 219,
Annual Volume 66 p. 37
1,3-DIMETHYL-3-METHOXY-4-PHENYLAZETIDINONE
Submitted by: Lous S. Hegedus, Michael A. McGuire, and Lisa M. Schultze
Published in Collective Volume 8 p. 216,
Annual Volume 65 p. 140
3,3-DIMETHYL-1,5-DIPHENYLPENTANE-1,5-DIONE
Submitted by: Koichi Narasaka
Published in Collective Volume 8 p. 210,
Annual Volume 65 p. 12
(S)-N,N-DIMETHYL-N'-(1-tert-BUTOXY-3-METHYL-2-BUTYL)FORMAMIDINE
Submitted by: Daniel A. Dickman, Michael Boes, and Albert I. Meyers
Published in Collective Volume 8 p. 204,
Annual Volume 67 p. 52
(R)-(−)-N,N-DIETHYL-(E)-CITRONELLALENAMINE AND (R)-(+)-CITRONELLAL VIA ISOMERIZATION OF N,N-DIETHYLGERANYLAMINE OR N,N-DIETHYLNERYLAMINE
Submitted by: Kazuhide Tani, Tsuneaki Yamagata, Sei Otsuka, Hidenori Kumobayashi, and Susumu Akutagawa
Published in Collective Volume 8 p. 183,
Annual Volume 67 p. 33
REARRANGEMENT OF 4-ARYL-4-HYDROXY-2,3-DIALKOXYCYCLOBUTENONES TO ANNULATED HYDROQUINONES AND QUINONES: 5,6-DIETHOXYBENZOFURAN-4,7-DIONE
Submitted by: S. T. Perri, P. Rice, and H. W. Moore
Published in Collective Volume 8 p. 179,
Annual Volume 69 p. 220
PREPARATION AND THREE-CARBON + TWO-CARBON CYCLOADDITION OF CYCLOPROPENONE 1,3-PROPANEDIOL KETAL: 5,5-DICYANO-4-PHENYL-2-CYCLOPENTEN-1-ONE 1,3-PROPANEDIOL KETAL
Submitted by: Dale L. Boger, Christine E. Brotherton, and Gunda I. Georg
Published in Collective Volume 8 p. 173,
Annual Volume 65 p. 32
1,4-DI-O-ALKYL THREITOLS FROM TARTARIC ACID: 1,4-DI-O-BENZYL-L-THREITOL
Submitted by: Eugene A. Mash, Keith A. Nelson, Shawne Van Deusen, and Susan B. Hemperly
Published in Collective Volume 8 p. 155,
Annual Volume 68 p. 92
TRIPLE-BOND ISOMERIZATIONS: 2- TO 9-DECYN-1-OL
Submitted by: Suzanne R. Abrams and Angela C. Shaw
Published in Collective Volume 8 p. 146,
Annual Volume 66 p. 127
HOFMANN REARRANGEMENT UNDER MILDLY ACIDIC CONDITIONS USING [I,I-BIS(TRIFLUOROACETOXY)]IODOBENZENE: CYCLOBUTYLAMINE HYDROCHLORIDE FROM CYCLOBUTANECARBOXAMIDE
Submitted by: Merrick R. Almond, Julie B. Stimmel, E. Alan Thompson, and G. Marc Loudon
Published in Collective Volume 8 p. 132,
Annual Volume 66 p. 132
PALLADIUM-CATALYZED COUPLING OF VINYL TRIFLATES WITH ORGANOSTANNANES: 4-tert-BUTYL-1-VINYLCYCLOHEXENE AND 1-(4-tert-BUTYLCYCLOHEXEN-1-YL)-2-PROPEN-1-ONE
Submitted by: William J. Scott, G. T. Crisp, and J. K. Stille
Published in Collective Volume 8 p. 97,
Annual Volume 68 p. 116
tert-BUTYL ACETOTHIOACETATE AND ITS USE IN SYNTHESIS: 3-ACETYL-4-HYDROXY-5,5-DIMETHYLFURAN-2(4H)-ONE
Submitted by: Christina M. J. Fox and Steven V. Ley
Published in Collective Volume 8 p. 71,
Annual Volume 66 p. 108
(R)-(+)- AND (S)-(−)-2,2'-BIS(DIPHENYLPHOSPHINO)-1,1'-BINAPHTHYL (BINAP)
Submitted by: Hidemasa Takaya, Susumu Akutagawa, and Ryoji Noyori
Published in Collective Volume 8 p. 57,
Annual Volume 67 p. 20
MIXED HIGHER-ORDER CYANOCUPRATE-INDUCED EPOXIDE OPENINGS: 1-BENZYLOXY-4-PENTEN-2-OL
Submitted by: Bruce H. Lipshutz, Robert Moretti, and Robert Crow
Published in Collective Volume 8 p. 33,
Annual Volume 69 p. 80
(S)-(−)-1-AMINO-2-METHOXYMETHYLPYRROLIDINE (SAMP) AND (R)-(+)-1-AMINO-2-METHOXYMETHYLPYRROLIDINE (RAMP), VERSATILE CHIRAL AUXILIARIES
Submitted by: Dieter Enders, Peter Fey, and Helmut Kipphardt
Published in Collective Volume 8 p. 26,
Annual Volume 65 p. 173
TRIS(DIMETHYLAMINO)SULFONIUM DIFLUOROTRIMETHYLSILICATE
Submitted by: William J. Middleton
Published in Collective Volume 7 p. 528,
Annual Volume 64 p. 221
cis-N-TOSYL-3-METHYL-2-AZABICYCLO[3.3.0]OCT-3-ENE
Submitted by: Louis S. Hegedus, Michael S. Holden, and James M. McKearin
Published in Collective Volume 7 p. 501,
Annual Volume 62 p. 48
PHENYL VINYL SULFONE AND SULFOXIDE
Submitted by: Leo A. Paquette and Richard V. C. Carr
Published in Collective Volume 7 p. 453,
Annual Volume 64 p. 157
ENANTIOSELECTIVE ADDITION OF BUTYLLITHIUM IN THE PRESENCE OF THE CHIRAL COSOLVENT DDB: (R)-( + )-1-PHENYL-1-PENTANOL
Submitted by: Dieter Seebach and August Hidber
Published in Collective Volume 7 p. 447,
Annual Volume 61 p. 42
TOSYLHYDRAZONE SALT PYROLYSES: PHENYLDIAZOMETHANES
Submitted by: Xavier Creary
Published in Collective Volume 7 p. 438,
Annual Volume 64 p. 207
α-tert-ALKYLATION OF KETONES: 2-tert-PENTYLCYCLOPENTANONE
Submitted by: M. T. Reetz, I. Chatziiosifidis, F. Hübner, and H. Heimbach
Published in Collective Volume 7 p. 424,
Annual Volume 62 p. 95
ASYMMETRIC HYDROGENATION OF KETOPANTOYL LACTONE: D-(−)-PANTOYL LACTONE
Submitted by: I. Ojima, T. Kogure, and Y. Yoda
Published in Collective Volume 7 p. 417,
Annual Volume 63 p. 18
2-METHYL-2-(TRIMETHYLSILOXY)PENTAN-3-ONE
Submitted by: Steven D. Young, Charles T. Buse, and Clayton H. Heathcock
Published in Collective Volume 7 p. 381,
Annual Volume 63 p. 79
(S)-8a-METHYL-3,4,8,8a-TETRAHYDRO-1,6(2H, 7H)-NAPHTHALENEDIONE
Submitted by: Paul Buchschacher, A. Fürst, and J. Gutzwiller
Published in Collective Volume 7 p. 368,
Annual Volume 63 p. 37
METHYL PHENYLACETYLACETATE FROM PHENYLACETYL CHLORIDE AND MELDRUM'S ACID
Submitted by: Y. Oikawa, T. Yoshioka, K. Sugano, and Osamu Yonemitsu
Published in Collective Volume 7 p. 359,
Annual Volume 63 p. 198
PREPARATION OF LOW-HALIDE METHYLLITHIUM
Submitted by: Michael J. Lusch, William V. Phillips, Ronald F. Sieloff, Glenn S. Nomura, and Herbert O. House
Published in Collective Volume 7 p. 346,
Annual Volume 62 p. 101
Z-1-IODOHEXENE
Submitted by: A. Alexakis, G. Cahiez, and J. F. Normant
Published in Collective Volume 7 p. 290,
Annual Volume 62 p. 1
SELECTIVE HYDROBORATION OF A 1,3,7-TRIENE: HOMOGERANIOL
Submitted by: Eric J. Leopold
Published in Collective Volume 7 p. 258,
Annual Volume 64 p. 164
HEXAMETHYL DEWAR BENZENE
Submitted by: Sami A. Shama and Carl C. Wamser
Published in Collective Volume 7 p. 256,
Annual Volume 61 p. 62
ALKYLATION OF THE ANION FROM BIRCH REDUCTION OF o-ANISIC ACID: 2-HEPTYL-2-CYCLOHEXENONE
Submitted by: D. F. Taber, B. P. Gunn, and I-Ching Chiu
Published in Collective Volume 7 p. 249,
Annual Volume 61 p. 59
ADDITION OF AN ETHYLCOPPER COMPLEX TO 1-OCTYNE: (E)-5-ETHYL-1,4-UNDECADIENE
Submitted by: Ramnath S. Iyer and Paul Helquist
Published in Collective Volume 7 p. 236,
Annual Volume 64 p. 1
(2SR,3RS)-2,4-DIMETHYL-3-HYDROXYPENTANOIC ACID
Submitted by: B. Bal, C. T. Buse, K. Smith, and Clayton H. Heathcock
Published in Collective Volume 7 p. 185,
Annual Volume 63 p. 89
DIASTEREOSELECTIVE α-ALKYLATION OF β-HYDROXYCARBOXYLIC ESTERS THROUGH ALKOXIDE ENOLATES: DIETHYL (2S, 3R)-(+)-3-ALLYL-2-HYDROXYSUCCINATE FROM DIETHYL (S)-( − )-MALATE
Submitted by: Dieter Seebach, Johannes Aebi, and Daniel Wasmuth
Published in Collective Volume 7 p. 153,
Annual Volume 63 p. 109
CYCLOBUTENE
Submitted by: J. Salaün and A. Fadel
Published in Collective Volume 7 p. 117,
Annual Volume 64 p. 50
PREPARATION OF THIOL ESTERS: S-tert-BUTYL CYCLOHEXANECARBOTHIOATE AND S-tert-BUTYL 3α,7α,12α-TRIHYDROXY-5β-CHOLANE-24-THIOATE
Submitted by: Gary O. Spessard, Wan Kit Chan, and S. Masamune
Published in Collective Volume 7 p. 81,
Annual Volume 61 p. 134
REDUCTIVE CLEAVAGE OF VINYL PHOSPHORODIAMIDATES: 17β-tert-BUTOXY-Gα-ANDROST-2-ENE
Submitted by: Robert E. Ireland, Thomas H. O'Neil, and Glen L. Tolman
Published in Collective Volume 7 p. 66,
Annual Volume 61 p. 116
CHIRAL MEDIA FOR ASYMMETRIC SOLVENT INDUCTIONS. (S,S)-( + )-1,4-BIS(DIMETHYLAMINO)-2,3-DIMETHOXYBUTANE FROM (R,R)-( + )-DIETHYL TARTRATE
Submitted by: Dieter Seebach, Hans-Otto Kalinowski, Werner Langer, Gerhard Crass, and Eva-Maria Wilka
Published in Collective Volume 7 p. 41,
Annual Volume 61 p. 24
REDUCTIVE COUPLING OF CARBONYLS TO ALKENES: ADAMANTYLIDENEADAMANTANE
Submitted by: Michael P. Fleming and John E. McMurry
Published in Collective Volume 7 p. 1,
Annual Volume 60 p. 113
3-TRIMETHYLSILYL-3-BUTEN-2-ONE: A MICHAEL ACCEPTOR
Submitted by: Robert K. Boeckman, David M. Blum, Bruce Ganem, and Neil Halvey
Published in Collective Volume 6 p. 1033,
Annual Volume 58 p. 152
3,5,5-TRIMETHYL-2-(2-OXOPROPYL)-2-CYCLOHEXEN-1-ONE
Submitted by: Z. Valenta and H. J. Liu
Published in Collective Volume 6 p. 1024,
Annual Volume 57 p. 113
ALDEHYDES FROM sym-TRITHIANE: n-PENTADECANAL
Submitted by: D. Seebach and A. K. Beck
Published in Collective Volume 6 p. 869,
Annual Volume 51 p. 39
HIGHLY REACTIVE MAGNESIUM FOR THE PREPARATION OF GRIGNARD REAGENTS: 1-NORBORNANECARBOXYLIC ACID
Submitted by: Reuben D. Rieke, Stephen E. Bales, Phillip M. Hudnall, Timothy P. Burns, and Graham S. Poindexter
Published in Collective Volume 6 p. 845,
Annual Volume 59 p. 85
NUCLEOPHILIC ACYLATION WITH DISODIUM TETRACARBONYLFERRATE: METHYL 7-OXOHEPTANOATE AND METHYL 7-OXOÖCTANOATE
Submitted by: Richard G. Finke, and Thomas N. Sorrell
Published in Collective Volume 6 p. 807,
Annual Volume 59 p. 102
PREPARATION AND REDUCTIVE CLEAVAGE OF ENOL PHOSPHATES: 5-METHYLCOPROST-3-ENE
Submitted by: D. C. Muchmore
Published in Collective Volume 6 p. 762,
Annual Volume 52 p. 109
VINYL SULFIDES FROM THIOACETALS WITH COPPER(I) TRIFLUOROMETHANESULFONATE: (Z)-2-METHOXY-1-PHENYLTHIO-1,3-BUTADIENE
Submitted by: Theodore Cohen, Robert J. Ruffner, David W. Shull, Elaine R. Fogel, and J. R. Falck
Published in Collective Volume 6 p. 737,
Annual Volume 59 p. 202
1,6-METHANO[10]ANNULENE
Submitted by: E. Vogel, W. Klug, and A. Breuer
Published in Collective Volume 6 p. 731,
Annual Volume 54 p. 11
REACTION OF ARYL HALIDES WITH π-ALLYLNICKEL HALIDES: METHALLYLBENZENE
Submitted by: Martin F. Semmelhack and Paul M. Helquist
Published in Collective Volume 6 p. 722,
Annual Volume 52 p. 115
3-TRIMETHYLSILYL-3-BUTEN-2-ONE AS MICHAEL ACCEPTOR FOR CONJUGATE ADDITION-ANNELATION: cis-4,4a,5,6,7,8-HEXAHYDRO-4a,5-DIMETHYL-2(3H)-NAPHTHALENONE
Submitted by: Robert K. Boeckman, David M. Blum, and Bruce Ganem
Published in Collective Volume 6 p. 666,
Annual Volume 58 p. 158
ETHYL 5β-CHOLEST-3-ENE-5-ACETATE
Submitted by: R. E. Ireland and D. J. Dawson
Published in Collective Volume 6 p. 584,
Annual Volume 54 p. 74
ESTERIFICATION OF CARBOXYLIC ACIDS WITH TRIALKYLOXONIUM SALTS: ETHYL AND METHYL 4-ACETOXYBENZOATES
Submitted by: Douglas J. Raber, Patrick Gariano, Jr, Albert O. Brod, Anne L. Gariano, and Wayne C. Guida
Published in Collective Volume 6 p. 576,
Annual Volume 56 p. 59
DEMETHYLATION OF METHYL ARYL ETHERS: 4-ETHOXY-3-HYDROXYBENZALDEHYDE
Submitted by: Robert E. Ireland and David M. Walba
Published in Collective Volume 6 p. 567,
Annual Volume 56 p. 44
NUCLEOPHILIC α-sec-AMINOALKYLATION: 2-(DIPHENYLHYDROXYMETHYL)PYRROLIDINE
Submitted by: D. Enders, R. Pieter, B. Renger, and D. Seebach
Published in Collective Volume 6 p. 542,
Annual Volume 58 p. 113
AROMATIC HYDROCARBONS FROM AROMATIC KETONES AND ALDEHYDES: 1,1-DIPHENYLETHANE
Submitted by: Sharon D. Lipsky and Stan S. Hall
Published in Collective Volume 6 p. 537,
Annual Volume 55 p. 7
DIMETHYL 2,3-PENTADIENEDIOATE
Submitted by: T. A. Bryson and T. M. Dolak
Published in Collective Volume 6 p. 505,
Annual Volume 57 p. 62
N,N-DIMETHYL-5β-CHOLEST-3-ENE-5-ACETAMIDE
Submitted by: R. E. Ireland and D. J. Dawson
Published in Collective Volume 6 p. 491,
Annual Volume 54 p. 77
DIAZO TRANSFER BY MEANS OF PHASE-TRANSFER CATALYSIS: DI-tert-BUTYL DIAZOMALONATE
Submitted by: Henry J. Ledon
Published in Collective Volume 6 p. 414,
Annual Volume 59 p. 66
CATALYTIC OSMIUM TETROXIDE OXIDATION OF OLEFINS: cis-1,2-CYCLOHEXANEDIOL
Submitted by: V. VanRheenen, D. Y. Cha, and W. M. Hartley
Published in Collective Volume 6 p. 342,
Annual Volume 58 p. 43
ONE-CARBON RING EXPANSION OF CYCLOALKANONES TO CONJUGATED CYCLOALKENONES: 2-CYCLOHEPTEN-1-ONE
Submitted by: Yoshihiko Ito, Shotaro Fujii, Masashi Nakatuska, Fumio Kawamoto, and Takeo Saegusa
Published in Collective Volume 6 p. 327,
Annual Volume 59 p. 113
CYCLIC KETONES FROM 1,3-DITHIANE: CYCLOBUTANONE
Submitted by: D. Seebach and A. K. Beck
Published in Collective Volume 6 p. 316,
Annual Volume 51 p. 76
PREPARATION OF CYANO COMPOUNDS USING ALKYLALUMINUM INTERMEDIATES: 1-CYANO-6-METHOXY-3,4-DIHYDRONAPHTHALENE
Submitted by: W. Nagata, M. Yoshioka, and M. Murakami
Published in Collective Volume 6 p. 307,
Annual Volume 52 p. 96
5β-CHOLEST-3-ENE-5-ACETALDEHYDE
Submitted by: R. E. Ireland and D. J. Dawson
Published in Collective Volume 6 p. 298,
Annual Volume 54 p. 71
SULFIDE SYNTHESIS IN PREPARATION OF UNSYMMETRICAL DIALKYL DISULFIDES: sec-BUTYL ISOPROPYL DISULFIDE
Submitted by: M. E. Alonso and H. Aragona
Published in Collective Volume 6 p. 235,
Annual Volume 58 p. 147
PHOTOCHEMICAL RING CONTRACTION OF 2-ETHOXYPYRROLIN-5-ONES TO CYCLOPROPANONE DERIVATIVES: tert-BUTYL N-(1-ETHOXYCYCLOPROPYL)CARBAMATE
Submitted by: Geoffrey C. Crockett and Tad H. Koch
Published in Collective Volume 6 p. 226,
Annual Volume 59 p. 132
OXIDATION OF ALCOHOLS BY METHYL SULFIDE – N-CHLOROSUCCINIMIDE – TRIETHYLAMINE: 4-tert-BUTYLCYCLOHEXANONE
Submitted by: E. J. Corey, C. U. Kim, and P. F. Misco
Published in Collective Volume 6 p. 220,
Annual Volume 58 p. 122
POLYMERIC CARBODIIMIDE. MOFFAT OXIDATION: 4-tert-BUTYLCYCLOHEXANONE
Submitted by: Ned M. Weinshenker, Chah M. Shen, and Jack Y. Wong
Published in Collective Volume 6 p. 218,
Annual Volume 56 p. 99
N-ALKYLINDOLES FROM THE ALKYLATION OF SODIUM INDOLIDE IN HEXAMETHYLPHOSPHORIC TRIAMIDE: 1-BENZYLINDOLE
Submitted by: George M. Rubottom and John C. Chabala
Published in Collective Volume 6 p. 106,
Annual Volume 54 p. 60
DIELS-ALDER ADDITION OF PERCHLOROBENZYNE: BENZOBARRELENE
Submitted by: Neil J. Hales, Harry Heaney, John H. Hollinshead, and Pritpal Singh
Published in Collective Volume 6 p. 82,
Annual Volume 59 p. 71
ALDEHYDES FROM 4,4-DIMETHYL-2-OXAZOLINE AND GRIGNARD REAGENTS: o-ANISALDEHYDE
Submitted by: R. S. Brinkmeyer, E. W. Collington, and A. I. Meyers
Published in Collective Volume 6 p. 64,
Annual Volume 54 p. 42
TERTIARY ALCOHOLS FROM HYDROCARBONS BY OZONATION ON SILICA GEL: 1-ADAMANTANOL
Submitted by: Zvi Cohen, Haim Varkony, Ehud Keinan, and Yehuda Mazur
Published in Collective Volume 6 p. 43,
Annual Volume 59 p. 176
1,2-DIMERCAPTOBENZENE
Submitted by: Aldo Ferretti
Published in Collective Volume 5 p. 419,
Annual Volume 42 p. 54
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