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1
Large-Scale Amino-Hydroxylation Using Tethered Nitreniums
Shyam Sathyamoorthi
Org. Synth. 2025, 102,
494
DOI: 10.15227/orgsyn.102.0494
Checked by: Theodor Elvebak and Christopher D. Vanderwal
2
Preparation of N-tert-Butylbenzenesulfinimidoyl Chloride
Teruaki Mukaiyama, Yasuo Nakamura, and Jun-ichi Matsuo
Org. Synth. 2025, 102,
477
DOI: 10.15227/orgsyn.102.0477
Checked by: Daniel W. Zuschlag and Dirk Trauner
3
Oxidative Nitrogen Atom Insertion into Cyclopentenones
Bence B. Botlik and Bill Morandi
Org. Synth. 2025, 102,
465
DOI: 10.15227/orgsyn.102.0465
Checked by: Maud T. H. Tregear, Anna J. Passmore, and Darren J. Dixon
4
Synthesis of Abietatriene via Nitrogen Deletion
Julia L. Driscoll, Carys E. Obertone, Liao Chen, and Mark D. Levin
Org. Synth. 2025, 102,
442
DOI: 10.15227/orgsyn.102.0442
Checked by: Yu Chen and Pauline Chiu
5
Hydrosilylation of Propiolate Esters
Allison M. Clark, Giulianna Miseo, and Neil K. Garg
Org. Synth. 2025, 102,
428
DOI: 10.15227/orgsyn.102.0428
Checked by: Seamus Higgins and Christopher Vanderwal
6
Acid-Mediated Hydroaminomethylation of Unactivated Alkenes
Uros Vezonik, Paolo Piacentini and Nuno Maulide
Org. Synth. 2025, 102,
414
DOI: 10.15227/orgsyn.102.0414
Checked by: Anagha Veluthanath Nair and M. Kevin Brown
7
Large-Scale Alkene Dimesyloxylation
Shyam Sathyamoorthi
Org. Synth. 2025, 102,
398
DOI: 10.15227/orgsyn.102.0398
Checked by: Hin Yu Kenneth Huang, Yu Chen, and Pauline Chiu
8
Synthesis of meta-Substituted Benzenes via Mo-Catalyzed Intermolecular Deoxygenative Coupling of Ynones and Allylic Amines
Yi-Zhe Yu, Gang Fang, Hong-Yi Su, and Chun-Xiang Zhuo
Org. Synth. 2025, 102,
381
DOI: 10.15227/orgsyn.102.0381
Checked by: Yanyao Liu and Kevin Campos
9
Synthesis of α-Aryl Ketones via the Nickel-Catalyzed Hydroacylation of Aryl Alkenes with Aroyl Fluorides
Yoonho Lee, Yujin Jung, Seonhwa Choo, and Kwangmin Shin
Org. Synth. 2025, 102,
367
DOI: 10.15227/orgsyn.102.0367
Checked by: Nicholas Cowper and Nathan Ide
10
Preparation of tBu-MsFluind-Br
Lucas Wagner and Josep Cornella
Org. Synth. 2025, 102,
350
DOI: 10.15227/orgsyn.102.0350
Checked by: Szymon Maciej Kosc, Katherine Clark, and Darren Dixon
11
Synthesis of 6-Methoxy-2-methyl-2-(4-methylpent-3-en-1-yl)chroman-4-one via Kabbe Condensation
Stephen A. Chamness, Emily F. Traficante, Trenton R. Vogel, and Corinna S. Schindler
Org. Synth. 2025, 102,
335
DOI: 10.15227/orgsyn.102.0335
Checked by: Max Neumann and Tehshik Yoon
12
Synthesis of gem-Difluoroalkenes through Ramberg-Bäcklund Reaction of Alkyltriflones
Motoo Ohtsuka, Yasuyo Tahara-Tezuka, Yuuki Maekawa, Cathleen M. Crudden, and Masakazu Nambo
Org. Synth. 2025, 102,
315
DOI: 10.15227/orgsyn.102.0315
Checked by: Nikolaos Skoulikas, Lorenz Erlbacher and Nuno Maulide
13
OS Techniques
Glass Cannula for Bulb-to-Bulb Cold Transfer
Kaylin N. Flesch, Tyler J. Fulton, Nathan Hart, and Brian M. Stoltz
Org. Synth. 2025, 102,
303
DOI: 10.15227/orgsyn.102.0303
Checked by: Mira Milic and Christopher D. Vanderwal
14
OS Techniques
Purification of Organic Compounds by Flash Column Chromatography
Benjamin D. Senzer, Cholapat Varongchayakul, Rick L. Danheiser*, Brian Daniels, and Vy M. Dong*
Org. Synth. 2025, 102,
276
DOI: 10.15227/orgsyn.102.0276
Checked by: Katerina Scotchburn and Sophie A. L. Rousseaux
15
Editorial
Announcing "OS Techniques" - A New Category of Articles in Organic Syntheses
Rick L. Danheiser
Org. Synth. 2025, 102,
273
DOI: 10.15227/orgsyn.102.0273
16
Rapid Access to Enantiopure Protected (R)-Paraconyl Alcohol
Haylie E. Hennigan, Namuunzul Otgontseren, and Elizabeth I. Parkinson
Org. Synth. 2025, 102,
251
DOI: 10.15227/orgsyn.102.0251
Checked by: David A. Petrone and Kevin R. Campos
17
Efficient Preparation of Chiral Hydroxylamines via Nickel-Catalyzed Asymmetric Hydrogenation of Oximes
Bowen Li, Jianzhong Chen, and Wanbin Zhang
Org. Synth. 2025, 102,
236
DOI: 10.15227/orgsyn.102.0236
Checked by: Greg Storer and Nathan Ide
18
Large-Scale Syntheses of Silanoxy-Tetrahydrofurans via Stereospecific [5,5]-Rearrangements of Silanol Epoxides
Silver Raju and Shyam Sathyamoorthi
Org. Synth. 2025, 102,
217
DOI: 10.15227/orgsyn.102.0217
Checked by: Nnamdi Akporji and Kevin Campos
19
Iodine-Catalyzed Stereospecific anti-Diamination of trans-?-Methylstyrene
Takeshi Sugiyama, Chiyuki Naito, and Satoshi Minakata
Org. Synth. 2025, 102,
203
DOI: 10.15227/orgsyn.102.0203
Checked by: Shun Kawano, Juri Sakata, and Hidetoshi Tokuyama
20
Synthesis of 1-(phenylsulfonyl)bicyclo[1.1.0]butane from Methyl Phenyl Sulfone and Epichlorohydrin
Joanna E. Muir, Myunggi Jung, and Vincent N. G. Lindsay
Org. Synth. 2025, 102,
185
DOI: 10.15227/orgsyn.102.0185
Checked by: Yu-Che Chang and M. Kevin Brown
21
Synthesis of Serine Derived Oxazolines Using a Molybdenum Dioxide Catalyst
Wyatt C. Powell, Garrett E. Evenson, and Maciej A. Walczak
Org. Synth. 2025, 102,
156
DOI: 10.15227/orgsyn.102.0156
Checked by: Zengsheng Yin and Pauline Chiu
22
Preparation of (Z)-N-Phenoxybenzimidoyl Chloride
Joseph P. Lokant, Ross M. Dare, and David A. Nagib
Org. Synth. 2025, 102,
143
DOI: 10.15227/orgsyn.102.0143
Checked by: Souvik Adak and M. Kevin Brown
23
C(sp2)-S Cross-Coupling Reactions with Adaptive Dynamic Homogeneous Catalysis: Synthesis of Ethyl 4-((3-Ethoxy-3-oxopropyl)thio)benzoate
Florence Babawale, Indrajit Ghosh, Burkhard König
Org. Synth. 2025, 102,
128
DOI: 10.15227/orgsyn.102.0128
Checked by: Nicholas D. D'Arcy-Evans, Evan Rutter, and Darren J. Dixon
24
Photoexcited Nitroarenes for the Anaerobic Cleavage of Alkenes
Lifeng Yin, Ben S. Kozloff, Ning Deng, Preya D. Persaud, Ajay H. Bansode, Dan E. Wise, Jenny S. Martinez, and Marvin Parasram
Org. Synth. 2025, 102,
114
DOI: 10.15227/orgsyn.102.0114
Checked by: Cailean Bonella, Alberto Ristache, and Darren Dixon
25
Large-Scale NaBr/Selectfluor Mediated Alcohol Oxidation: Conversion of (-)-Borneol into (-)-Camphor
Shyam Sathyamoorthi
Org. Synth. 2025, 102,
100
DOI: 10.15227/orgsyn.102.0100
Checked by: Sergio Armentia Matheu, Saad Shaaban, and Nuno Maulide
26
Copper-Catalyzed Suzuki-Miyaura Coupling of Unactivated Alkyl Halides with Arylborons
Yonglei Zhou, Jian Li, and Weilong Xie
Org. Synth. 2025, 102,
86
DOI: 10.15227/orgsyn.102.0086
Checked by: Kathryn M. Weber and Tehshik P. Yoon
27
A General Method for C-Alkylation of Nitroalkanes with Alkyl Halides: Nickel Photoredox Dual-Catalyzed C-Alkylation of Nitroalkanes
Sina Rezazadeh, Allyssa M. Conner, and Donald A. Watson
Org. Synth. 2025, 102,
64
DOI: 10.15227/orgsyn.102.0064
Checked by: Neetu Sharma and M. Kevin Brown
28
Preparation of 1,3-Dihydroxyphenazine
Trevor Dzwiniel, Emma Markun, James A. Kaduk, Aaron Hollas, Krzystof Pupek, and Nicholas Boaz
Org. Synth. 2025, 102,
45
DOI: 10.15227/orgsyn.102.0045
Checked by: Uros Vezonik, Florian Doubek and Nuno Maulide
29
Synthesis of Borane-Ammonia and its Application in the Titanium Tetrachloride Catalyzed Reduction of Carboxylic Acids, Including N-Protected Amino Acids
Henry J. Hamann, Abdulkhaliq A. Alawaed, and P. Veeraraghavan Ramachandran
Org. Synth. 2025, 102,
19
DOI: 10.15227/orgsyn.102.0019
Checked by: Gwyndaf A. Oliver, Konstantin Gunther and Nuno Maulide
30
Sharpless Epoxidation of Divinyl Carbinol
Klaus-Peter Ruhmann, Paula Mora, and Dirk Trauner
Org. Synth. 2025, 102,
1
DOI: 10.15227/orgsyn.102.0001
Checked by: Aaron L. Featherston, Nathan Ide, and Seble Wagaw
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