A Publication
of Reliable Methods
for the Preparation
of Organic Compounds
Annual Volume
Volume 99 (2022)
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Synthesis of Triphenylene via the Palladium-Catalyzed Annulation of Benzyne
Katie A. Spence, Milauni M. Mehta, and Neil K. Garg
Org. Synth. 2022, 99, 174
DOI: 10.15227/orgsyn.099.0174
Checked by: Hridaynath Bhattacharjee and Cathleen Crudden

Reaction scheme
Synthesis of Phenanthridinones via the Palladium-Catalyzed Annulation of Benzyne
Dominick C. Witkowski, Luca McDermott, and Neil K. Garg
Org. Synth. 2022, 99, 159
DOI: 10.15227/orgsyn.099.0159
Checked by: Russell D. Cink and Seble Wagaw

Reaction scheme
Organocatalytic Dimerization of Succinaldehyde
Steven H. Bennett and Varinder K. Aggarwal
Org. Synth. 2022, 99, 139
DOI: 10.15227/orgsyn.099.0139
Checked by: Tufan K. Mukhopadhyay and Dirk Trauner

Reaction scheme
Chelsea R. Wilson, Evan F. W. Chen, Austia O. Puckett, and Fraser Hof
Org. Synth. 2022, 99, 125
DOI: 10.15227/orgsyn.099.0125
Checked by: Marc Poirier and Kevin Campos

Reaction scheme
Discussion Addendum for: Preparation of 1,1-Difluoroallenes by Difluorovinylidenation of Carbonyl Compounds
Kohei Fuchibe and Junji Ichikawa
Org. Synth. 2022, 99, 113
DOI: 10.15227/orgsyn.099.0113
Original Article: Org. Synth. 2016, 93, 352

Reaction scheme
Preparation of MIDA Anhydride and Reaction with Boronic Acids
Peng-Jui Chen, Aidan M. Kelly, Daniel J. Blair, and Martin D. Burke
Org. Synth. 2022, 99, 92
DOI: 10.15227/orgsyn.099.0092
Checked by: Jack Hayward Cooke and Richmond Sarpong

Reaction scheme
Preparation of a Donor-Acceptor Stenhouse Adduct (DASA): 5-((2Z,4E)-5-(Diethylamino)-2-hydroxypenta-2,4-dien-1-ylidene)-2,2-dimethyl-1,3-dioxane-4,6-dione
Friedrich Stricker, Julie Peterson, and Javier Read de Alaniz
Org. Synth. 2022, 99, 79
DOI: 10.15227/orgsyn.099.0079
Checked by: Feng Peng and Kevin Campos

Reaction scheme
Discussion Addendum for: Asymmetric Michael Reaction of Aldehydes and Nitroalkenes
Yujiro Hayashi
Org. Synth. 2022, 99, 68
DOI: 10.15227/orgsyn.099.0068
Original Article: Org. Synth. 2017, 94, 252

Reaction scheme
A Convenient Method for the Removal of Tetrabutylammonium Salts from Desilylation Reactions
Luca McDermott, Dominick C. Witkowski, and Neil K. Garg
Org. Synth. 2022, 99, 53
DOI: 10.15227/orgsyn.099.0053
Checked by: Philipp Spieß, Daniel Kaiser and Nuno Maulide

Reaction scheme
Transition-Metal-Free Synthesis of an Aryl Boronate Ester through Base-Mediated Boryl Substitution of an Aryl Halide with a Silylborane
Ryosuke Shishido1a and Hajime Ito
Org. Synth. 2022, 99, 39
DOI: 10.15227/orgsyn.099.0039
Checked by: Praveen Kumar Gajula, Gopal Sirasani and Chris Senanayake

Reaction scheme
Preparation of N-Formylamides by Oxidative Cleavage of N-Acylaminoacids
Nick Kilenyi
Org. Synth. 2022, 99, 29
DOI: 10.15227/orgsyn.099.0029
Checked by: Miran Lemmerer, Manuel Schupp, and Nuno Maulide

Reaction scheme
Synthesis of Alkylboronic Esters from Alkyl Iodides
Qianyi Liu, Hao Liang, Shangyong Zhou, Lei Zhang, Jianxin Yang, Yunxing Yin, Yang Yang, Di Qiu and Fanyang Mo
Org. Synth. 2022, 99, 15
DOI: 10.15227/orgsyn.099.0015
Checked by: Jordan Thompson and Sarah Reisman

Reaction scheme
Synthesis of [(R)-DTBM-SEGPHOS]NiCl2 for the Enantioselective Acetal Formation from N-Propanoyl-1,3-Thiazinane-2-thione and Trimethyl Orthoformate
Stuart C. D. Kennington, Pedro Romea, and Fèlix Urpí
Org. Synth. 2022, 99, 1
DOI: 10.15227/orgsyn.099.0001
Checked by: Zhaobin Han and Kuiling Ding

Reaction scheme

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Board of Editors
All procedures and characterization data in OrgSyn are peer-reviewed and checked for reproducibility in the laboratory of a member of the Board of Editors