A Publication
of Reliable Methods
for the Preparation
of Organic Compounds
Annual Volume
Volume 94 (2017)
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Preparation of N-Trifluoromethylthiosaccharin: A Shelf-Stable Electrophilic Reagent for Trifluoromethylthiolation
Jiansheng Zhu, Chunhui Xu, Chunfa Xu, and Qilong Shen
Org. Synth. 2017, 94, 217
DOI: 10.15227/orgsyn.094.0217
Checked by: Jon Lorenz and Chris Senanayake

Reaction scheme
4-Cyano-2-methoxybenzenesulfonyl Chloride
Elliott D. Bayle, Niall Igoe, and Paul V. Fish
Org. Synth. 2017, 94, 198
DOI: 10.15227/orgsyn.094.0198
Checked by: Kevin Gayler, Aoi Kimishima, and John Wood

Reaction scheme
Jeremy Nugent and Brett D. Schwartz
Org. Synth. 2017, 94, 184
DOI: 10.15227/orgsyn.094.0184
Checked by: Luke E. Hanna and Sarah Reisman

Reaction scheme
Fragment Coupling and Formation of Quaternary Carbons by Visible-Light Photoredox Catalyzed Reaction of tert-Alkyl Hemioxalate Salts and Michael Acceptors
Christopher R. Jamison, Yuriy Slutskyy, and Larry E. Overman
Org. Synth. 2017, 94, 167
DOI: 10.15227/orgsyn.094.0167
Checked by: Anthony Y. Chen, Eric R. Welin, Tyler J. Fulton, and Brian Stoltz

Reaction scheme
Hongwen Luo, Dengke Ma, and Shengming Ma
Org. Synth. 2017, 94, 153
DOI: 10.15227/orgsyn.094.0153
Checked by: Carl A. Busacca and Chris Senanayake

Reaction scheme
Dirhodium (II) tetrakis[N-4-bromo-1,8-naphthoyl-(S)-tert-leucinate]
Hélène Lebel*, Henri Piras, and Johan Bartholoméüs
Org. Synth. 2017, 94, 136
DOI: 10.15227/orgsyn.094.0136
Checked by: David Stephens and Richmond Sarpong

Reaction scheme
Rhodium(I)-catalyzed Allenic Pauson–Khand Reaction
Joseph E. Burchick. Jr., Sarah M. Wells, and Kay M. Brummond
Org. Synth. 2017, 94, 123
DOI: 10.15227/orgsyn.094.0123
Checked by: Arthur Han and Sarah E. Reisman

Reaction scheme
Synthesis of Allenyl Mesylate by a Johnson-Claisen Rearrangement. Preparation of 3-(((tert-butyldiphenyl-silyl)oxy)methyl)penta-3,4-dien-1-yl methanesulfonate
Joseph E. Burchick. Jr., Sarah M. Wells, and Kay M. Brummond
Org. Synth. 2017, 94, 109
DOI: 10.15227/orgsyn.094.0109
Checked by: Susan M. Stevenson and Sarah E. Reisman

Reaction scheme
(Z)-Enol p-Tosylate Derived from Methyl Acetoacetate: A Useful Cross-coupling Partner for the Synthesis of Methyl (Z)-3-Phenyl (or Aryl)-2-butenoate
Yuichiro Ashida, Hidefumi Nakatsuji, and Yoo Tanabe
Org. Synth. 2017, 94, 93
DOI: 10.15227/orgsyn.094.0093
Checked by: Yuji Suzuki and Keisuke Suzuki

Reaction scheme
Practical Syntheses of [2,2′-bipyridine]bis[3,5-difluoro-2-[5-(trifluoromethyl)-2-pyridinyl]phenyl]iridium(III)hexafluorophosphate, [Ir{dF(CF3)ppy}2(bpy)]PF6 and [4,4′-bis(tert-butyl)-2,2′-bipyridine]bis[3,5-difluoro-2-[5-(trifluoromethyl)-2-pyridinyl]phenyl]iridium(III)hexafluorophosphate, [Ir{dF(CF3)ppy}2(dtbbpy)]PF6
Martins S. Oderinde and Jeffrey W. Johannes
Org. Synth. 2017, 94, 77
DOI: 10.15227/orgsyn.094.0077
Checked by: Nadide Hazal Avcı, Chase Olsson, Brandon Nelson, and Mohammad Movassaghi

Reaction scheme
Palladium-catalyzed External-CO-Free Reductive Carbonylation of Bromoarenes
Hideyuki Konishi, Masataka Fukuda, Tsuyoshi Ueda, and Kei Manabe
Org. Synth. 2017, 94, 66
DOI: 10.15227/orgsyn.094.0066
Checked by: Jordan C. Beck and Sarah E. Reisman

Reaction scheme
Ugi Multicomponent Reaction
André Boltjes, Haixia Liu, Haiping Liu, and Alexander Dömling
Org. Synth. 2017, 94, 54
DOI: 10.15227/orgsyn.094.0054
Checked by: Emma L. Baker-Tripp and Neil K. Garg

Reaction scheme
Site-Selective C-H Fluorination of Pyridines and Diazines with AgF2
Patrick S. Fier and John F. Hartwig
Org. Synth. 2017, 94, 46
DOI: 10.15227/orgsyn.094.0046
Checked by: Matthew G. Beaver, Christopher J. Borths, and Margaret M. Faul

Reaction scheme
Continuous Flow Hydration of Pyrazine-2-carbonitrile in a Manganese Dioxide Column Reactor
Claudio Battilocchio, Shing-Hing Lau, Joel M. Hawkins, and Steven V. Ley
Org. Synth. 2017, 94, 34
DOI: 10.15227/orgsyn.094.0034
Checked by: Frederic Buono, Andrew Brusoe and Chris Senanayake

Reaction scheme
Preparation of Diisopropylammonium Bis(catecholato)cyclohexylsilicate
Kingson Lin, Christopher B. Kelly, Matthieu Jouffroy, and Gary A. Molander
Org. Synth. 2017, 94, 16
DOI: 10.15227/orgsyn.094.0016
Checked by: Andrés García-Domínguez, Estíbaliz Merino, and Cristina Nevado

Reaction scheme
Preparation of Aryl Alkyl Ketenes
Nicholas D. Staudaher, Joseph Lovelace, Michael P. Johnson, and Janis Louie
Org. Synth. 2017, 94, 1
DOI: 10.15227/orgsyn.094.0001
Checked by: Sheng Guo and Dawei Ma

Reaction scheme

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Board of Editors
All procedures and characterization data in OrgSyn are peer-reviewed and checked for reproducibility in the laboratory of a member of the Board of Editors