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1
Synthesis of Methyl 1-Formylcyclopropanecarboxylate utilizing Ti-Claisen Condensation
Yuichiro Ashida, Satomi Kajimoto, Hidefumi Nakatsuji, and Yoo Tanabe
Org. Synth. 2016, 93,
286
DOI: 10.15227/orgsyn.093.0286
Checked by: Bryon K. Anderson, Yu-Wen Huang, and John L. Wood
2
Synthesis of α-Carboline
Linli He, Shawn P. Allwein, Benjamin J. Dugan, Kyle W. Knouse, Gregory R. Ott, and Craig A. Zificsak
Org. Synth. 2016, 93,
272
DOI: 10.15227/orgsyn.093.0272
Checked by: Kevin Kou and Richmond Sarpong
3
Potassium tert-Butoxide–Catalyzed Dehydrogenative Cross-Coupling of Heteroarenes with Hydrosilanes
Anton A. Toutov, Wen-Bo Liu, Brian M. Stoltz, and Robert H. Grubbs
Org. Synth. 2016, 93,
263
DOI: 10.15227/orgsyn.093.0263
Checked by: Jose M. Medina and Neil K. Garg
4
Synthesis of 1-Iodopropyne
Samuel G. Bartko, James Deng, and Rick L. Danheiser
Org. Synth. 2016, 93,
245
DOI: 10.15227/orgsyn.093.0245
Checked by: Joshua Cox and John L. Wood
5
Oxyboration: Synthesis of Borylated Benzofurans
Darius J. Faizi, Nicole A. Nava, Mohammad Al-Amin, and Suzanne A. Blum
Org. Synth. 2016, 93,
228
DOI: 10.15227/orgsyn.093.0228
Checked by: Nicholas A. Weires and Neil K. Garg
6
Preparation of 1,5-Dioxaspiro[5.5]undecan-3-one
Robert A. Craig, II, Russell C. Smith, Beau P. Pritchett, Benzi I. Estipona, and Brian M. Stoltz
Org. Synth. 2016, 93,
210
DOI: 10.15227/orgsyn.093.0210
Checked by: Marcel Weiss and Mohammad Movassaghi
7
Preparation of Methyl 1,2,3,4-tetra-O-acetyl-β-D-glucopyranuronate
Aisling Ní Cheallaigh, Garrett T. Potter, John M. Gardiner, and Gavin J. Miller
Org. Synth. 2016, 93,
200
DOI: 10.15227/orgsyn.093.0200
Checked by: Michal Achmatowicz and Margaret Faul
8
Visible Light Photocatalysis of Radical Cation Diels–Alder Cycloadditions: Preparation of Tris(2,2’-bipyrazyl) Ruthenium(II) Bis(tetrakis(3,5-bis(trifluoromethyl)phenyl)borate)
Shane D. Lies, Shishi Lin, and Tehshik P. Yoon
Org. Synth. 2016, 93,
178
DOI: 10.15227/orgsyn.093.0178
Checked by: Stanley Chang and Richmond Sarpong
9
Copper-catalyzed Cyanation of Alkenyl Iodides
Antoine Nitelet, Sara Zahim, Cédric Theunissen, Alexandre Pradal, and Gwilherm Evano
Org. Synth. 2016, 93,
163
DOI: 10.15227/orgsyn.093.0163
Checked by: Sidney M. Wilkerson-Hill and Huw M. L. Davies
10
Trifluoromethylation of Aryl Iodides Catalyzed by the Copper(I)-Phen Complex
Naoto Shimizu, Hideaki Kondo, Masahiro Oishi, Kenichi Fujikawa, Kazuki Komoda, and Hideki Amii
Org. Synth. 2016, 93,
147
DOI: 10.15227/orgsyn.093.0147
Checked by: Mina Nakhla and John L. Wood
11
Photochemical Benzannulation of N-Phosphoryl Ynamides and α-Diazo Ketones in Continuous Flow
John M. Read, Yu-Pu Wang, and Rick L. Danheiser
Org. Synth. 2016, 93,
127
DOI: 10.15227/orgsyn.093.0127
Checked by: Christian Ebner and Erick M. Carreira
12
Intermolecular [2+2] Cycloaddition of Alkynes with Alkenes Catalyzed by Gold(I)
M. Elena de Orbe, and Antonio M. Echavarren
Org. Synth. 2016, 93,
115
DOI: 10.15227/orgsyn.093.0115
Checked by: Giulia Rusconi, Estíbaliz Merino and Cristina Nevado
13
Synthesis of 1-Bromopyrene and 1-Pyrenecarbaldehyde
Matthias Schulze, Alexander Scherer, Colin Diner, and Rik R. Tykwinski
Org. Synth. 2016, 93,
100
DOI: 10.15227/orgsyn.093.0100
Checked by: Jeffrey D. Mighion and Huw M. L. Davies
14
Enantioselective Synthesis of α-Bromonitroalkanes for Umpolung Amide Synthesis: Preparation of tert-Butyl ((1R)-1-(4-(benzyloxy)phenyl)-2-bromo-2-nitroethyl)carbamate
Victoria T. Lim, Sergey V. Tsukanov, Amanda B. Stephens, and Jeffrey N. Johnston
Org. Synth. 2016, 93,
88
DOI: 10.15227/orgsyn.093.0088
Checked by: Fabian Konrad, Estíbaliz Merino and Cristina Nevado
15
Enantioselective Synthesis of α,α-Disubstituted Lactones via a Chiral Brønsted Acid Catalyzed Intramolecular Cyclization
Jennifer E. Wilent, Ghassan Qabaja, and Kimberly S. Petersen
Org. Synth. 2016, 93,
75
DOI: 10.15227/orgsyn.093.0075
Checked by: Bo Qu and Chris H. Senanayake
16
Trichloroboron-promoted Deprotection of Phenolic Benzyl Ether Using Pentamethylbenzene as a Non Lewis-Basic Cation Scavenger
Shun Okaya, Keiichiro Okuyama, Kentaro Okano, and Hidetoshi Tokuyama
Org. Synth. 2016, 93,
63
DOI: 10.15227/orgsyn.093.0063
Checked by: Brandon Nelson, Nicholas Garcia, and Mohammad Movassaghi
17
Nickel-Catalyzed Synthesis of Ketones from Alkyl Halides and Acid Chlorides: Preparation of Ethyl 4-Oxododecanoate
Alexander C. Wotal, Donald C. Batesky, and Daniel J. Weix
Org. Synth. 2016, 93,
50
DOI: 10.15227/orgsyn.093.0050
Checked by: Yongda Zhang and Chris H. Senanayake
18
Erratum for: Titanium-Mediated Addition of Silyl Dienol Ethers to Electrophilic Glycine: 4-Ketopipecolic Acid Hydrochloride
Clarisse Mühlemann, Peter Hartmann, and Jean-Pierre Obrecht
Org. Synth. 2016, 93,
37
DOI: 10.15227/orgsyn.093.0037
19
Synthesis of 5-(Hydroxymethyl)furfural (HMF)
Svilen P. Simeonov, Jaime A. S. Coelho, and Carlos A. M. Afonso
Org. Synth. 2016, 93,
29
DOI: 10.15227/orgsyn.093.0029
Checked by: Mengyang Fan and Dawei Ma
20
Preparation of 2-(2-(Dicyclohexylphosphino)phenyl)-1-methyl-1H-indole (CM-phos)
Shun Man Wong, On Ying Yuen, Pui Ying Choy, Chau Ming So, and Fuk Yee Kwong
Org. Synth. 2016, 93,
14
DOI: 10.15227/orgsyn.093.0014
Checked by: Takumi Fukazawa and Keisuke Suzuki
21
DIBALH-Mediated Reductive Ring-Expansion Reaction of Cyclic Ketoxime
Taku Imaizumi, Kentaro Okano, and Hidetoshi Tokuyama
Org. Synth. 2016, 93,
1
DOI: 10.15227/orgsyn.093.0001
Checked by: Lang-Tin Xu and Dawei Ma
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Board of Editors
Margaret M. Faul
Amgen, Inc
Cristina Nevado
University of Zurich
Richmond Sarpong
University of California, Berkeley
Chris Senanayake
Boehringer Ingelheim Pharmaceuticals
John L. Wood
Baylor University
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