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Volume 92 (2015)
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Ruthenium-Catalyzed Direct Oxidative Alkenylation of Arenes through Twofold C–H Bond Functionalization in Water: Synthesis of Ethyl (E)-3-(2-Acetamido-4-methylphenyl)acrylate
Lianhui Wang, Karsten Rauch, Alexander V. Lygin, Sergei I. Kozhushkov and Lutz Ackermann
Org. Synth. 2015, 92, 131
DOI: 10.15227/orgsyn.092.0131
Checked by: William Trieu and Margaret Faul

Reaction scheme
Copper(II) Triflate as Additive in Low Loading Au(I)-Catalyzed Hydroalkylation of Unactivated Alkenes
Weizhen Fang, Marc Presset, Amandine Guérinot, Christophe Bour, Sophie Bezzenine-Lafollée, and Vincent Gandon
Org. Synth. 2015, 92, 117
DOI: 10.15227/orgsyn.092.0117
Checked by: Pavel K. Elkin and Viresh H. Rawal

Reaction scheme
Preparation of N-(Boc)-Allylglycine Methyl Ester Using a Zinc-mediated, Palladium-catalyzed Cross-coupling Reaction
N. D. Prasad Atmuri and William D. Lubell
Org. Synth. 2015, 92, 103
DOI: 10.15227/orgsyn.092.0103
Checked by: Jean-Nicolas Desrosiers, Nizar Haddad, and Chris H. Senanayake

Reaction scheme
Preparation of Mono-Cbz Protected Guanidines
Kihyeok Kwon, Travis J. Haussener and Ryan E. Looper
Org. Synth. 2015, 92, 91
DOI: 10.15227/orgsyn.092.0091
Checked by: Joshua N. Payette and Mohammad Movassaghi

Reaction scheme
Palladium-catalyzed β -Selective C(sp3)-H Arylation of N-Boc-Piperidines
Anthony Millet and Olivier Baudoin
Org. Synth. 2015, 92, 76
DOI: 10.15227/orgsyn.092.0076
Checked by: Louis C. Morrill and Richmond Sarpong

Reaction scheme
Ligand-Accelerated ortho-C-H Olefination of Phenylacetic Acids
Keary M. Engle, Navid Dastbaravardeh, Peter S. Thuy-Boun, Dong-Hui Wang, Aaron C. Sather, and Jin-Quan Yu
Org. Synth. 2015, 92, 58
DOI: 10.15227/orgsyn.092.0058
Checked by: Sandeep N. Raikar and Huw M. L. Davies

Reaction scheme
Enantioselective Reductive Syn-Aldol Reactions of 4-Acryloylmorpholine: Preparation of (2R, 3S)-3-Hydroxy-2-methyl-1-morpholino-5-phenylpentan-1-one
Jason R. Abbott, Christophe Allais, and William R. Roush
Org. Synth. 2015, 92, 38
DOI: 10.15227/orgsyn.092.0038
Checked by: Simon Krautwald, Simon Breitler, and Erick M. Carreira

Reaction scheme
Preparation of Crystalline (Diisopinocampheyl)borane
Jason R. Abbott, Christophe Allais, and William R. Roush
Org. Synth. 2015, 92, 26
DOI: 10.15227/orgsyn.092.0026
Checked by: Simon Krautwald, Simon Breitler, and Erick M. Carreira

Reaction scheme
Synthesis of 4,4-Dimethoxybut-1-yne
James Deng, Yu-Pu Wang, and Rick L. Danheiser
Org. Synth. 2015, 92, 13
DOI: 10.15227/orgsyn.092.0013
Checked by: Yutaka Kobayashi and John L. Wood

Reaction scheme
Iridium-Catalyzed Enantioselective Allylic Vinylation with Potassium Alkenyltrifluoroborates
James Y. Hamilton, David Sarlah, and Erick M. Carreira
Org. Synth. 2015, 92, 1
DOI: 10.15227/orgsyn.092.0001
Checked by: Wen-bo (Boger) Liu, Seo-Jung Han, and Brian M. Stoltz

Reaction scheme

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Board of Editors
All procedures and characterization data in OrgSyn are peer-reviewed and checked for reproducibility in the laboratory of a member of the Board of Editors