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Volume 94 (2017)
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1
N-Methoxy-N-methylcyanoformamide
Jeremy Nugent and Brett D. Schwartz
Org. Synth. 2017, 94, 184
DOI: 10.15227/orgsyn.094.0184
Checked by: Luke E. Hanna and Sarah Reisman

Reaction scheme
2
Fragment Coupling and Formation of Quaternary Carbons by Visible-Light Photoredox Catalyzed Reaction of tert-Alkyl Hemioxalate Salts and Michael Acceptors
Christopher R. Jamison, Yuriy Slutskyy, and Larry E. Overman
Org. Synth. 2017, 94, 167
DOI: 10.15227/orgsyn.094.0167
Checked by: Anthony Y. Chen, Eric R. Welin, Tyler J. Fulton, and Brian Stoltz

Reaction scheme
3
Buta-2,3-dien-1-ol
Hongwen Luo, Dengke Ma, and Shengming Ma
Org. Synth. 2017, 94, 153
DOI: 10.15227/orgsyn.094.0153
Checked by: Carl A. Busacca and Chris Senanayake

Reaction scheme
4
Dirhodium (II) tetrakis[N-4-bromo-1,8-naphthoyl-(S)-tert-leucinate]
Hélène Lebel*, Henri Piras, and Johan Bartholoméüs
Org. Synth. 2017, 94, 136
DOI: 10.15227/orgsyn.094.0136
Checked by: David Stephens and Richmond Sarpong

Reaction scheme
5
Rhodium(I)-catalyzed Allenic Pauson–Khand Reaction
Joseph E. Burchick. Jr., Sarah M. Wells, and Kay M. Brummond
Org. Synth. 2017, 94, 123
DOI: 10.15227/orgsyn.094.0123
Checked by: Arthur Han and Sarah E. Reisman

Reaction scheme
6
Synthesis of Allenyl Mesylate by a Johnson-Claisen Rearrangement. Preparation of 3-(((tert-butyldiphenyl-silyl)oxy)methyl)penta-3,4-dien-1-yl methanesulfonate
Joseph E. Burchick. Jr., Sarah M. Wells, and Kay M. Brummond
Org. Synth. 2017, 94, 109
DOI: 10.15227/orgsyn.094.0109
Checked by: Susan M. Stevenson and Sarah E. Reisman

Reaction scheme
7
(Z)-Enol p-Tosylate Derived from Methyl Acetoacetate: A Useful Cross-coupling Partner for the Synthesis of Methyl (Z)-3-Phenyl (or Aryl)-2-butenoate
Yuichiro Ashida, Hidefumi Nakatsuji, and Yoo Tanabe
Org. Synth. 2017, 94, 93
DOI: 10.15227/orgsyn.094.0093
Checked by: Yuji Suzuki and Keisuke Suzuki

Reaction scheme
8
Practical Syntheses of [2,2′-bipyridine]bis[3,5-difluoro-2-[5-(trifluoromethyl)-2-pyridinyl]phenyl]iridium(III)hexafluorophosphate, [Ir{dF(CF3)ppy}2(bpy)]PF6 and [4,4′-bis(tert-butyl)-2,2′-bipyridine]bis[3,5-difluoro-2-[5-(trifluoromethyl)-2-pyridinyl]phenyl]iridium(III)hexafluorophosphate, [Ir{dF(CF3)ppy}2(dtbbpy)]PF6
Martins S. Oderinde and Jeffrey W. Johannes
Org. Synth. 2017, 94, 77
DOI: 10.15227/orgsyn.094.0077
Checked by: Nadide Hazal Avcı, Chase Olsson, Brandon Nelson, and Mohammad Movassaghi

Reaction scheme
9
Palladium-catalyzed External-CO-Free Reductive Carbonylation of Bromoarenes
Hideyuki Konishi, Masataka Fukuda, Tsuyoshi Ueda, and Kei Manabe
Org. Synth. 2017, 94, 66
DOI: 10.15227/orgsyn.094.0066
Checked by: Jordan C. Beck and Sarah E. Reisman

Reaction scheme
10
Ugi Multicomponent Reaction
André Boltjes, Haixia Liu, Haiping Liu, and Alexander Dömling
Org. Synth. 2017, 94, 54
DOI: 10.15227/orgsyn.094.0054
Checked by: Emma L. Baker-Tripp and Neil K. Garg

Reaction scheme
11
Site-Selective C-H Fluorination of Pyridines and Diazines with AgF2
Patrick S. Fier and John F. Hartwig
Org. Synth. 2017, 94, 46
DOI: 10.15227/orgsyn.094.0046
Checked by: Matthew G. Beaver, Christopher J. Borths, and Margaret M. Faul

Reaction scheme
12
Continuous Flow Hydration of Pyrazine-2-carbonitrile in a Manganese Dioxide Column Reactor
Claudio Battilocchio, Shing-Hing Lau, Joel M. Hawkins, and Steven V. Ley
Org. Synth. 2017, 94, 34
DOI: 10.15227/orgsyn.094.0034
Checked by: Frederic Buono, Andrew Brusoe and Chris Senanayake

Reaction scheme
13
Preparation of Diisopropylammonium Bis(catecholato)cyclohexylsilicate
Kingson Lin, Christopher B. Kelly, Matthieu Jouffroy, and Gary A. Molander
Org. Synth. 2017, 94, 16
DOI: 10.15227/orgsyn.094.0016
Checked by: Andrés García-Domínguez, Estíbaliz Merino, and Cristina Nevado

Reaction scheme
14
Preparation of Aryl Alkyl Ketenes
Nicholas D. Staudaher, Joseph Lovelace, Michael P. Johnson, and Janis Louie
Org. Synth. 2017, 94, 1
DOI: 10.15227/orgsyn.094.0001
Checked by: Sheng Guo and Dawei Ma

Reaction scheme

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Board of Editors
All procedures and characterization data in OrgSyn are peer-reviewed and checked for reproducibility in the laboratory of a member of the Board of Editors
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