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1
3-Component Approach to 1,5-Dihydro-2H-pyrrol-2-one Heterocycles
Nicholas P. Massaro and Joshua G. Pierce
Org. Synth. 2023, 100,
418
DOI: 10.15227/orgsyn.100.0418
Checked by: Colin Knus, Jorge A. González, and Cristina Nevado
2
Preparation of (S)-5,5ʹ,6,6ʹ,7,7ʹ,8,8ʹ-Octahydro-1,1'-bi-2-naphthol [(S)-H8BINOL]
Jiong Chen, Yuan-Yuan Zhu and Shuang-Xi Gu
Org. Synth. 2023, 100,
404
DOI: 10.15227/orgsyn.100.0404
Checked by: Jacob Waldman and Kevin Campos
3
Preparation of (S)-3,3ʹ-Bis(1-pyrrolidinylmethyl)-5,5ʹ,6,6ʹ, 7,7ʹ,8,8ʹ-octahydro-1,1'-bi-2-naphthol
Yu Hong, Yuan-Yuan Zhu, and Shuang-Xi Gu
Org. Synth. 2023, 100,
394
DOI: 10.15227/orgsyn.100.0394
Checked by: Chibueze I. Onyeagusi and Kevin Campos
4
Preparation of 4-(5-(p-Tolyl)-3-(trifluoromethyl)-1H-pyrazol-1-yl)benzenesulfonyl fluoride (ArSO2F)
Lucas Wagner, Clément Ghiazza and Josep Cornella
Org. Synth. 2023, 100,
382
DOI: 10.15227/orgsyn.100.0382
Checked by: Haoqi Zhang, Daniel Kaiser and Nuno Maulide
5
Preparation of Pyrylium Tetrafluoroborate (Pyry-BF4)
Alejandro Gómez-Palomino, Clément Ghiazza, Julia Busch, Lucas Wagner and Josep Cornella
Org. Synth. 2023, 100,
361
DOI: 10.15227/orgsyn.100.0361
Checked by: Thomas Leischner, Benjamin Thomas Jones, and Nuno Maulide
6
Synthesis of 4-Phenylpyrrolidin-2-one via an Aza-Baeyer-Villiger Rearrangement
Mike Ong, Marlene Arnold, and Johannes M. Wahl
Org. Synth. 2023, 100,
347
DOI: 10.15227/orgsyn.100.0347
Checked by: Shashwati Paul and M. Kevin Brown
7
Stereoselective Synthesis of (E)-Vinylstannanes from Alkynes via Hydroboration and Transmetalation
Ruiyang Guo and Rick L. Danheiser
Org. Synth. 2023, 100,
327
DOI: 10.15227/orgsyn.100.0327
Checked by: Stanna K. Dorn and Sarah E. Reisman
8
Synthesis of a Furoindoline Scaffold via an Interrupted Fischer Indolization
Georgia M. Scherer, Jordan Gonzalez, Laura G. Wonilowicz, and Neil K. Garg
Org. Synth. 2023, 100,
304
DOI: 10.15227/orgsyn.100.0304
Checked by: Yu-Hin Ho, Zengsheng Yin, and Pauline Chiu
9
Discussion Addendum for: Indium-Catalyzed Heteroaryl-Heteroaryl Bond Formation through Nucleophilic Aromatic Substitution: Preparation of 2-Methyl-3-(thien-2-yl)-1H-indole
Teruhisa Tsuchimoto
Org. Synth. 2023, 100,
287
DOI: 10.15227/orgsyn.100.0287
10
Visible-light-mediated Oxidative Debenzylation of 3-O-Benzyl-1,2:5,6-di-O-isopropylidene-α-D-glucofuranose
Amiera Madani, Eric T. Sletten, Cristian Cavedon, Peter H. Seeberger, and Bartholomäus Pieber
Org. Synth. 2023, 100,
271
DOI: 10.15227/orgsyn.100.0271
Checked by: Kevin Lee and Dirk Trauner
11
Synthesis of 2-Phenyl-4,6-bis(trifluoromethyl)pyridine via NH4I/Na2S2O4-Mediated Cyclization of Ketoxime Acetates
Huawen Huang, Zhenhua Xu, and Guo-Jun Deng
Org. Synth. 2023, 100,
248
DOI: 10.15227/orgsyn.100.0248
Checked by: Hisahiro Morozumi, Koichi Hagiwara, and Masayuki Inoue
12
Visible-Light-Promoted C-S Cross-Coupling Reaction for Synthesis of Aromatic Thioethers
Yingjun Lan, Junhua Xu, Chern-Hooi Lim, Garret M. Miyake, and Bin Liu
Org. Synth. 2023, 100,
234
DOI: 10.15227/orgsyn.100.0234
Checked by: Luca McDermott, Zachary Walters, and Neil K. Garg
13
Synthesis of Potassium 5-Bromopentyltrifluoroborate via Hydroboration of a Haloalkene
Sarah J. Burke, Latifah M. Alhthlol, James M. Gamrat, Giulia Mancini, Christopher L. Orme, Jacqueline R. Santhouse, Dylan T. Tomares, and John W. Tomsho
Org. Synth. 2023, 100,
218
DOI: 10.15227/orgsyn.100.0218
Checked by: Philip Boehm and Sarah E. Reisman
14
Synthesis of Phenols from Benzoic Acids
Wenzhang Xiong, Rui Wang, Zhengqiang Liu, Feng Peng, Ralph Zhao, and Wenbo H. Liu
Org. Synth. 2023, 100,
199
DOI: 10.15227/orgsyn.100.0199
Checked by: Martina Drescher, Saad Shaaban and Nuno Maulide
15
Synthesis of Enantioenriched NH-Sulfoximines by NH Transfer to Sulfoxides Using Ammonium Carbamate and (Diacetoxyiodo)benzene
Edward L. Briggs, Tsz-Kan Ma, Zhenhao Zhong, Arianna Tota, Leonardo Degennaro, Renzo Luisi and James A. Bull
Org. Synth. 2023, 100,
186
DOI: 10.15227/orgsyn.100.0186
Checked by: Ellie Plachinski and Tehshik Yoon
16
Synthesis of a 2,5-Bis(tert-butyldimethylsilyloxy)furan and its Reaction with Benzyne
Jessica E. Budwitz and Christopher G. Newton
Org. Synth. 2023, 100,
159
DOI: 10.15227/orgsyn.100.0159
Checked by: Dave J. Charboneau, Jordan K. Thompson, and Sarah E. Reisman
17
α-Oxamination of Amides via Electrophilic Activation
Miran Lemmerer, Ján Matyašovský, Roberto Tinelli and Nuno Maulide
Org. Synth. 2023, 100,
136
DOI: 10.15227/orgsyn.100.0136
Checked by: Colin Knus, Jaime Martín, Jorge A. González, and Cristina Nevado
18
N-(Benzyloxy)-N-(pivaloyloxy)-4-(trifluoromethyl)-benzamide
Kathleen J. Berger, Balu D. Dherange, Megan Morales, Julia L. Driscoll, A. Kaan Tarhan, and Mark D. Levin
Org. Synth. 2023, 100,
113
DOI: 10.15227/orgsyn.100.0113
Checked by: Yinuo Zheng and Pauline Chiu
19
α-Arylation of Cyclopentanones by Palladium/Enamine Cooperative Catalysis
Yibin Xue, Arjuna Parsad, and Guangbin Dong
Org. Synth. 2023, 100,
99
DOI: 10.15227/orgsyn.100.0099
Checked by: Jaejoong Han, Masanori Nagatomo, and Masayuki Inoue
20
Synthesis of Diethyl (1-Diazo-2-oxopropyl)phosphonate
Cholapat Varongchayakul and Rick L. Danheiser
Org. Synth. 2023, 100,
84
DOI: 10.15227/orgsyn.100.0084
Checked by: Michael D. Clift, Steve M. Richter, Zhe Wang, and Seble Wagaw
21
Preparation of N-Boc-3-methylpyrrole via Anionic Rearrangement
Daniel P. Graeff, Noah J. Sims, Quentin R. Savage, Richard K. Jackson, III, Amy C. Jackson, Danielle M. Lawson, Madelyn R. Wixom, and John L. Wood
Org. Synth. 2023, 100,
61
DOI: 10.15227/orgsyn.100.0061
Checked by: Yuya Shiga, Haruka Fujino, and Masayuki Inoue
22
Synthesis of NH-Sulfoximines from Sulfides Using Ammonium Carbamate and (Diacetoxyiodo)benzene to Transfer NH and O
Arianna Tota, Mauro Spennacchio, Edward L. Briggs, Tsz-Kan Ma, Zhenhao Zhong, Leonardo Degennaro, James A. Bull and Renzo Luisi
Org. Synth. 2023, 100,
48
DOI: 10.15227/orgsyn.100.0048
Checked by: Ellie Plachinski and Tehshik Yoon
23
Discussion Addendum for: Rh(I)-Catalyzed Allenic Pauson-Khand Reaction
Eric D. Deihl, Fatemeh Haghighi, and Kay M. Brummond
Org. Synth. 2023, 100,
29
DOI: 10.15227/orgsyn.100.0029
24
Preparation of Highly-Substituted Pyridines via Diels-Alder Reactions of Vinylallenes and Tosyl Cyanide
Nathan H. Faialaga, Christian Gomez, Samuel G. Bartko, Philipp Natho, and Rick L. Danheiser
Org. Synth. 2023, 100,
4
DOI: 10.15227/orgsyn.100.0004
Checked by: Christopher C. Nawrat and Kevin R. Campos
25
Editorial
Introducing Volume 100 of Organic Syntheses
Rick L. Danheiser
Org. Synth. 2023, 100,
1
DOI: 10.15227/orgsyn.100.0001
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