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1
Iridium-Catalyzed Reductive Coupling of Grignard Reagents and Tertiary Amides
Pablo Gabriel, Lan-Gui Xie, and Darren J. Dixon
Org. Synth. 2019, 96,
511
DOI: 10.15227/orgsyn.096.0511
Checked by: Karli R. Holman and Sarah E. Reisman
2
Synthesis of 5-Hydroxy-4-methoxy-2-methylpyrylium Trifluoromethanesulfonate from Kojic acid
Nana B. Agyemang and Ryan P. Murelli
Org. Synth. 2019, 96,
494
DOI: 10.15227/orgsyn.096.0494
Checked by: Richard K. Jackson III and John L. Wood
3
Discussion Addendum for: Fluorobis(phenylsulfonyl)methane (FBSM)
Xanath Ispizua-Rodriguez, Vinayak Krishnamurti, Mathew Coe and G. K. Surya Prakash
Org. Synth. 2019, 96,
474
DOI: 10.15227/orgsyn.096.0474
4
Preparation of 2,4,5,6-Tetra(9H-carbazol-9-yl)isophthalonitrile
Saskia M. Engle, Takisha R. Kirkner, and Christopher B. Kelly
Org. Synth. 2019, 96,
455
DOI: 10.15227/orgsyn.096.0455
Checked by: Shinsuke Shimizu, Koichi Hagiwara, and Masayuki Inoue
5
Facile Reduction of Amides Using Nickel Catalysis: Reduction of 12-Aminododecanolactam
Bryan J. Simmons, Melissa Ramirez, and Neil K. Garg
Org. Synth. 2019, 96,
436
DOI: 10.15227/orgsyn.096.0436
Checked by: Tsukasa Shimakawa, Koichi Hagiwara, and Masayuki Inoue
6
anti-1,2,2,3,4,4-Hexamethylphosphetane 1-Oxide
Trevor V. Nykaza, Julian C. Cooper, and Alexander T. Radosevich
Org. Synth. 2019, 96,
418
DOI: 10.15227/orgsyn.096.0418
Checked by: Robert-Cristian Raclea, Kyan A. D'Angelo, and Mohammad Movassaghi
7
Preparation of a Diisopropylselenophosphoramide Catalyst and its Use in Enantioselective Sulfenoetherification
Scott E. Denmark, Pavel Ryabchuk, Hyung Min Chi, and Anastassia Matviitsuk
Org. Synth. 2019, 96,
400
DOI: 10.15227/orgsyn.096.0400
Checked by: Michael Rombola and Sarah E. Reisman
8
(R)-N,N'-Dimethyl-1,1'-binaphthyldiamine
Scott E. Denmark and Pavel G. Ryabchuk
Org. Synth. 2019, 96,
382
DOI: 10.15227/orgsyn.096.0382
Checked by: Eric R. Welin and Brian M. Stoltz
9
Discussion Addendum for: Preparation of (R,R)-1,2:4,5-Diepoxypentane
Nicholas Sizemore and Scott D. Rychnovsky
Org. Synth. 2019, 96,
361
DOI: 10.15227/orgsyn.096.0361
10
Stereoselective Synthesis of (R)-((R)-1-Phenyl-2,2,2-trichloroethyl)2-(2-bromophenyl)aziridine-1-carboxylate
Hélène Lebel and Henri Piras
Org. Synth. 2019, 96,
351
DOI: 10.15227/orgsyn.096.0351
Checked by: Tony Z. Scott, Aniket Dehadrai, and Mohammad Movassaghi
11
Catalytic Enantioselective Addition of an In-Situ Prepared Aryltitanium Reagent to p-Chloroacetophenone: (R)-(+)-1-(4-Chlorophenyl)-1-m-tolylethanol
Yusuke Kobayashi, Atsushi Matsuda, Tomoya Ushimaru, and Toshiro Harada
Org. Synth. 2019, 96,
333
DOI: 10.15227/orgsyn.096.0333
Checked by: Jonathan Hughes and Kevin Campos
12
Preparation of (R)-3-(3,5-Bistrifluoromethylphenyl)-1,1'-bi-2-naphthol
Yusuke Kobayashi, Atsushi Matsuda, Tomoya Ushimaru, and Toshiro Harada
Org. Synth. 2019, 96,
312
DOI: 10.15227/orgsyn.096.0312
Checked by: Andrew J. Neel and Kevin Campos
13
Discussion Addendum for: Allylic Oxidation Catalyzed by Dirhodium(II) Tetrakis[ε-caprolactamate] of tert-Butyldimethylsilyl-protected trans-Dehydroandrosterone
Yong-Liang Su, Luca De Angelis and Michael P. Doyle
Org. Synth. 2019, 96,
300
DOI: 10.15227/orgsyn.096.0300
14
Three-Step Synthesis of 2-(Diiodomethyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane from Dichloromethane
Morgane Sayes, Guillaume Benoit, and André B. Charette
Org. Synth. 2019, 96,
277
DOI: 10.15227/orgsyn.096.0277
Checked by: Alexander R. Rovira and Richmond Sarpong
15
Preparation of 5-(Triisopropylalkynyl) dibenzo[b,d]thiophenium triflate
Bernd Waldecker, Kevin Kafuta, and Manuel Alcarazo
Org. Synth. 2019, 96,
258
DOI: 10.15227/orgsyn.096.0258
Checked by: Christopher C. Nawrat, Chuck Orella, Donald Bachert, and Kevin Campos
16
Synthesis of Chiral Diamine Ligands for Nickel-catalyzed Asymmetric Cross-couplings of Alkylchloroboronate Esters with Alkylzincs: (1R,2R)-N,N'-Dimethyl-1,2-bis(2-methylphenyl)-1,2-diaminoethane
Yusuke Masuda and Gregory C. Fu
Org. Synth. 2019, 96,
245
DOI: 10.15227/orgsyn.096.0245
17
Discussion Addendum for: Synthesis of Highly Enantiomerically Enriched Amines by Asymmetric Transfer Hydrogenation of N-(tert-Butylsulfinyl) Imines
Miguel Yus
Org. Synth. 2019, 96,
232
DOI: 10.15227/orgsyn.096.0232
18
Discussion Addendum for: Phosphine-Catalyzed [3 + 2] Annulation: Synthesis of Ethyl 5-(tert-Butyl)-2-phenyl-1-tosyl-3-pyrroline-3-carboxylate
Aslam C. Shaikh and Ohyun Kwon
Org. Synth. 2019, 96,
214
DOI: 10.15227/orgsyn.096.0214
19
Discussion Addendum for: Synthesis of Ynamides by Copper-Mediated Coupling of 1,1-Dibromo-1-alkenes with Nitrogen Nucleophiles. Preparation of 4-Methyl-N-(2-phenylethynyl)-N-(phenylmethyl)benzenesulfonamide
Cédric Theunissen,Pierre Thilmany, Mounsef Lahboub, Nicolas Blanchard and Gwilherm Evano
Org. Synth. 2019, 96,
195
DOI: 10.15227/orgsyn.096.0195
20
Discussion Addendum for: Preparation of Enantioenriched Homoallylic Primary Amines
Miguel Yus
Org. Synth. 2019, 96,
179
DOI: 10.15227/orgsyn.096.0179
21
Gold-Catalyzed Oxidative Coupling of Arenes and Arylsilanes
Chris Nottingham, Verity Barber, and Guy C. Lloyd-Jones
Org. Synth. 2019, 96,
150
DOI: 10.15227/orgsyn.096.0150
Checked by: Alexandre Genoux, Estíbaliz Merino, and Cristina Nevado
22
Synthesis of 4-Methylbenzoate(2ʹ,4ʹ,6ʹ-trimethoxy-phenyl)iodonium Tosylate
Thomas L. Seidl, Aaron Moment, Charles Orella, Thomas Vickery, and David R. Stuart
Org. Synth. 2019, 96,
137
DOI: 10.15227/orgsyn.096.0137
Checked by: Zhaobin Han and Kuiling Ding
23
Discussion Addendum for: Protection of Alcohols using 2-Benzyloxy-1-methylpyridinium Trifluoromethanesulfonate: Methyl (R)-(-)-3-Benzyloxy-2-methyl Propanoate
Harvey F. Fulo, Philip A. Albiniak, and Gregory B. Dudley
Org. Synth. 2019, 96,
124
DOI: 10.15227/orgsyn.096.0124
24
Discussion Addendum for: Phosphine-Catalyzed [4 + 2] Annulation: Synthesis of Ethyl 6-Phenyl-1-tosyl-1,2,5,6-tetrahydropyridine-3-carboxylate
Aslam C. Shaikh and Ohyun Kwon
Org. Synth. 2019, 96,
110
DOI: 10.15227/orgsyn.096.0110
25
Discussion Addendum for: Convenient Preparation of 3-Ethoxycarbonyl Benzofurans from Salicylaldehydes and Ethyl Diazoacetate
Mizzanoor Rahaman and M. Mahmun Hossain
Org. Synth. 2019, 96,
98
DOI: 10.15227/orgsyn.096.0098
26
Discussion Addendum for: The Direct Acyl-Alkylation of Arynes. Preparation of Methyl 2-(2-acetylphenyl)acetate
Austin C. Wright and Brian M. Stoltz
Org. Synth. 2019, 96,
80
DOI: 10.15227/orgsyn.096.0080
27
Synthesis of 2,3-Diaryl-2H-azirines via Cs2CO3-Mediated Cyclization of Ketoxime Acetates
Mi-Na Zhao and Zheng-Hui Guan
Org. Synth. 2019, 96,
66
DOI: 10.15227/orgsyn.096.0066
Checked by: Dirk Trauner and Julius R. Reyes
28
Discussion Addendum for: Lithium Amides as Homochiral Ammonia Equivalents for Conjugate Additions to α,β-Unsaturated Esters: Asymmetric Synthesis of (S)-β:Leucine
Stephen G. Davies, Ai M. Fletcher, Paul M. Roberts, and James E. Thomson
Org. Synth. 2019, 96,
53
DOI: 10.15227/orgsyn.096.0053
29
Nickel-Catalyzed Cross-Coupling of 2-Methoxynaphthalene with Methyl 4-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)benzoate
Yuki Kawashima, Takayuki Furukawa, Naoto Chatani* and Mamoru Tobisu
Org. Synth. 2019, 96,
36
DOI: 10.15227/orgsyn.096.0036
Checked by: Takumi Fukuda, Masanori Nagatomo, and Masayuki Inoue
30
Late-Stage Deoxyfluorination of Phenols with PhenoFluorMix
Junting Chen and Tobias Ritter
Org. Synth. 2019, 96,
16
DOI: 10.15227/orgsyn.096.0016
Checked by: Shota Nagasawa and Richmond Sarpong
31
Discussion Addendum for: 4-Nonylbenzoic Acid
Alois Fürstner
Org. Synth. 2019, 96,
1
DOI: 10.15227/orgsyn.096.0001
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